Polyelectrolyte laminated membrane
A technology of polymer electrolyte and membrane layer, which is applied in the direction of layered products, circuits, fuel cells, etc., and can solve problems such as unusable fuel cells and wrinkles
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[0110] (Production of Polymer Electrolyte Membrane)
[0111] As a polymer electrolyte membrane, it is fabricated as follows by [CF 2 CF 2 ] 0.812 -[CF 2 -CF(-O-(CF 2 ) 2 -SO 3 H)] 0.188 An electrolyte membrane composed of the shown perfluorosulfonic acid polymer (hereinafter referred to as "PFS").
[0112] First, as the precursor polymers of PFS, tetrafluoroethylene and CF 2 =CFO(CF 2 ) 2 -SO 2 F perfluorocarbon polymer (MI: 3.0). The precursor polymer was melt-extruded and molded to a thickness of about 50 μm, and the molded film was mixed with a reaction liquid containing 15 mass % potassium hydroxide, 30 mass % dimethyl sulfoxide and 55 mass % water at 60 ° C Contact for 4 hours to carry out hydrolysis treatment. Thereafter, the membrane was immersed in 60° C. water for 4 hours, and then immersed in 60° C. 2N hydrochloric acid aqueous solution for 3 hours, and the acid was washed away with ion-exchanged water to obtain a polymer electrolyte membrane.
[0113] ...
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