Core-shell USY@SBA-15 composite material as well as preparation method and application thereof
A composite material, core-shell technology, applied in chemical instruments and methods, hydrocarbon oil treatment, molecular sieve catalysts, etc., can solve the problem of difficulty in synthesizing core-shell USYSBA-15 composite materials, and shorten the hydrolysis time and shell layer. Controllable thickness and reduced assembly time
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[0035] Example 1:
[0036] (1) Under stirring, add 6.0 g TEOS to 14.0 g pH=2.8 HCl solution. After stirring at room temperature for 6 hours, the solution changed from a turbid liquid to a clear solution. Let it stand for 24 hours and set aside.
[0037] (2) Dissolve 1.21g P123 surfactant in 130 g 0.4 mol / L hydrochloric acid solution, add 2.38 g ground USY molecular sieve, stir for 10 min, and then add the TEOS pre-hydrolyzed solution prepared in (1), 30 Stir at constant temperature for 4 h at ℃.
[0038] (3) Adjust the pH of the reaction solution to 4.0 with ammonia water. (2) Crystallize at 100°C for 24 hours, filter, wash, dry, and calcinate at 550°C for 6 hours to obtain a core-shell structure USYSBA-15 with a shell thickness of 80 nm. 80) Materials.
Example Embodiment
[0039] Example 2:
[0040] (1) Under stirring, add 6.0 g TEOS to 14.0 g HCl solution with pH=2.8. After stirring at room temperature for 6 hours, the solution turns from a turbid liquid to a clear solution. Let it stand for 24 hours for later use.
[0041] (2) Dissolve 1.21 g P123 surfactant in 130 g 0.4 mol / L hydrochloric acid solution, add 3.55 g ground USY molecular sieve, stir for 10 min, and then add the TEOS pre-hydrolyzed solution prepared in (1), 30 Stir at constant temperature for 4 h at ℃.
[0042] (3) Adjust the pH of the reaction solution to 4.0 with ammonia. (2) Crystallize at 100 ℃ for 24 h, filter, wash, dry, and calcinate at 550 ℃ for 6 h to obtain a core-shell structure USYSBA-15 with a shell thickness of 60 nm. (60) Materials.
Example Embodiment
[0043] Example 3:
[0044] (1) Under stirring, add 6.0 g TEOS to 14.0 g pH=2.8 HCl solution. After stirring at room temperature for 6 hours, the solution changed from a turbid liquid to a clear solution. Let it stand for 24 hours and set aside.
[0045] (2) Dissolve 1.21g P123 surfactant in 130 g 0.4 mol / L hydrochloric acid solution, add 4.76 g ground USY molecular sieve, stir for 10 min, and then add the TEOS pre-hydrolyzed solution prepared in (1), 30 Stir at constant temperature for 4 h at ℃.
[0046] (3) Adjust the pH of the reaction solution to 4.0 with ammonia water, crystallize at 100 ℃ for 24 h, filter, wash, dry, and calcinate at 550 ℃ for 6 h to obtain a core-shell structure USYSBA-15 with a shell thickness of 30 nm (30) Materials.
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