Method for preparing fuel gas by burning biomass
A biomass and gas technology, which is applied in the manufacture of combustible gas, combustible gas purification, combustible gas purification/transformation, etc., can solve problems such as clogging of reaction tubes, and achieve the effect of increasing gas production rate and reducing tar content
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[0051] The preparation of the calcined dolomite catalyst is as follows: crush the dolomite, screen out particles with a particle size of 0.3-0.45 mm, and calcinate at a temperature of 900° C. for 4 hours.
[0052] The carbon nanotube (CNT) grafted Fe-NiO / TiO 2 The concrete preparation method of catalyst is as follows:
[0053] The first step, Fe-NiO / TiO 2 Preparation of catalyst, weigh 68g tetrabutyl titanate solution, add 377mL absolute ethanol and 26.75g nitric acid, stir to obtain solution A; 0.404gFe(NO 3 ) 3 9H 2 O,2.619g Ni(NO 3 )2·6H 2 O was dissolved in 215mL deionized water to obtain solution B. Add solution B dropwise to solution A, stir for 2h, let stand for 20h, and dry at 120°C. Raise the temperature to 500°C at a rate of 3°C / min, and roast for 3h. Preparation Fe-NiO / TiO 2 ;
[0054] In the second step, take the prepared Fe-NiO / TiO 2 10g is placed in a fluidized bed reactor, and the nitrogen flow rate is adjusted to 5L / min to fluidize the catalyst. The te...
Embodiment 1
[0063] The preparation of embodiment 1 calcined dolomite
[0064] Crush the dolomite, screen out particles with a particle size of 0.3-0.45mm, and calcinate at 900°C for 4 hours to obtain the product.
Embodiment 2
[0065] Example 2 Fe-NiO / TiO grafted with carbon nanotubes (CNT) 2 Catalyst preparation
[0066] The surface characteristics of the catalyst were analyzed by ASAP2010 specific surface and pore size analyzer (Micrometrics).
[0067]Weigh 68g tetrabutyl titanate solution, add 377mL absolute ethanol and 26.75g nitric acid, stir to obtain solution A; 0.404gFe(NO 3 ) 3 9H 2 O,2.619g Ni(NO 3 ) 2 ·6H 2 O was dissolved in 215mL deionized water to obtain solution B. Add solution B dropwise to solution A, stir for 2h, let stand for 20h, and dry at 120°C. Raise the temperature to 500°C at a rate of 3°C / min, and roast for 3h. Preparation Fe-NiO / TiO 2 , the prepared Fe-Ni / TiO 2 The comparative area is 63.0m 2 / g, take the prepared Fe-NiO / TiO 2 Put 10g of catalyst in a fluidized bed reactor, adjust the flow rate of nitrogen gas to 5L / min to fluidize the catalyst. Raise the temperature to 500°C, and after the temperature in the reactor is stabilized, feed acetylene gas into the reac...
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