Crude benzene hydrorefining process
A technology for hydrorefining and crude benzene, applied in the fields of hydrocarbons, chemical instruments and methods, organic chemistry, etc., can solve the problems of easy coking and clogging of the reaction system, high reaction temperature requirements, and many waste of raw materials, etc. Coking risk, stable reaction process, lower energy consumption and cost savings
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Embodiment 1
[0047] 1. The raw material is coking crude benzene, and its components and mass fractions are as follows:
[0048] Benzene: 75%, toluene: 13.9%, xylene: 2.24%, light component: 0.86%, heavy component: 8%, total sulfur content 6546.57ppm, total nitrogen content 899.3ppm.
[0049] 2. In this example, the reaction temperature of the liquid-phase catalytic prehydrogenation reaction is 140°C, the catalyst is Co-Mo, the volume ratio of hydrogen to oil is 500:1, and the volume space velocity is 3h -1 , pressure 2.8MPa;
[0050] The reaction temperature of the gas-phase catalytic prehydrogenation reaction is 190°C, the catalyst is Ni-Mo catalyst, the volume ratio of hydrogen to oil is 400:1, and the volume space velocity is 0.5h -1 , pressure 2.0MPa;
[0051] The reaction temperature of the main catalytic hydrogenation reaction is 270°C, the catalyst is Cr-Mo catalyst, the volume ratio of hydrogen to oil is 400:1, and the volume space velocity is 0.5h -1 , Pressure 2.0MPa.
[0052...
Embodiment 2
[0055] The present embodiment is operated by embodiment 1, difference is:
[0056] In this example, the reaction temperature of the liquid-phase catalytic prehydrogenation reaction is 130°C, the catalyst is Co-Mo, the volume ratio of hydrogen to oil is 300:1, and the volume space velocity is 0.1h -1 , pressure 2.4MPa;
[0057] The reaction temperature of the gas-phase catalytic prehydrogenation reaction is 210°C, the catalyst is Ni-Mo catalyst, the volume ratio of hydrogen to oil is 500:1, and the volume space velocity is 5h -1 , pressure 2.8MPa;
[0058] The reaction temperature of the main catalytic hydrogenation reaction is 290°C, the catalyst is Cr-Mo catalyst, the volume ratio of hydrogen to oil is 500:1, and the volume space velocity is 5h -1 , Pressure 2.8MPa.
[0059] After hydrogenation reaction:
[0060] The total sulfur content of the product is 0.2ppm and the total nitrogen content is less than 0.3ppm. The retention rate of aromatics in the liquid-phase catalyt...
Embodiment 3
[0062] The present embodiment is operated by embodiment 1, difference is:
[0063] In this example, the reaction temperature of the liquid-phase catalytic prehydrogenation reaction is 135°C, the catalyst is Co-Mo, the volume ratio of hydrogen to oil is 400:1, and the volume space velocity is 2h -1 , pressure 2.6MPa;
[0064] The reaction temperature of the gas-phase catalytic prehydrogenation reaction is 200°C, the catalyst is Ni-Mo catalyst, the volume ratio of hydrogen to oil is 450:1, and the volume space velocity is 3h -1 , pressure 2.6MPa;
[0065] The reaction temperature of the main catalytic hydrogenation reaction is 280°C, the catalyst is Cr-Mo catalyst, the volume ratio of hydrogen to oil is 450:1, and the volume space velocity is 3h -1 , Pressure 2.6MPa.
[0066] After hydrogenation reaction:
[0067] The total sulfur content of the product is 0.2ppm and the total nitrogen content is less than 0.3ppm. The retention rate of aromatics in the liquid-phase catalytic...
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