Anti-corrosion block rare earth-based metal glass and annealing method thereof
A base metal and corrosion-resistant technology, applied in the field of preparation of amorphous alloy materials, can solve problems such as weak resistance to crystallization, and achieve the effects of strong amorphous forming ability, increased corrosion resistance, and simple annealing process.
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Embodiment 1
[0040] According to the atomic percentage of 29.31% cerium, 21.83 lanthanum, 3.53 praseodymium, 7.08% samarium, 3.25% gadolinium, 25% cobalt and 10% aluminum (purity ≥ 99.5%, mass ratio), a total of 50g was weighed. Put the metal raw material in a copper mold cooled by circulating water, pass in 0.6MPa argon gas under vacuum conditions, and adjust the distance between the tungsten electrode and the metal raw material to be 1cm under the voltage of 380v; turn on the power, and start arcing the material ; Repeated melting 3 times to ensure that the alloy components are mixed evenly. Turn off the power, open the suction casting valve at the same time, control the pressure difference at 0.4MPa and start the suction casting to obtain a corrosion-resistant rare earth-based bulk metallic glass sample.
Embodiment 2
[0042] Put the corrosion-resistant rare earth-based metal glass sample prepared in Example 1 into a low-temperature atmosphere tube furnace (argon protection condition), keep it warm at 100°C for 1 hour, quickly take out the sample and put it into a beaker filled with water at 0°C middle. After the amorphous alloy sample is cooled, the corrosion-resistant rare earth-based bulk metallic glass is obtained. After detection, the alloy after annealing treatment is still completely amorphous.
Embodiment 3
[0044] Put the corrosion-resistant rare earth-based metal glass sample prepared in Example 1 into a low-temperature atmosphere tube furnace (argon protection condition), heat it at 100°C for 4 hours, quickly take out the sample and put it into a beaker filled with water at 0°C middle. After the amorphous alloy sample is cooled, the corrosion-resistant rare earth-based bulk metallic glass is obtained. After detection, the alloy after annealing treatment is still completely amorphous.
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