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crucible

一种坩埚、粉末的技术,应用在制造用于硅锭生产的坩埚领域,能够解决尚未取得成功等问题,达到改善寿命、高抗弯强度、高热传导率的效果

Inactive Publication Date: 2016-03-16
STEULER SOLAR
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] Apart from these attempts, the production of crucibles for silicon nitride, which are reusable and allow the production of high-quality silicon ingots, has not yet been successful

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0061] The mixture was prepared from silicon powder having a particle size of less than 10 microns and a particle size of less than 45 microns (weight ratio 1 : 1 ) together with about 25% by weight of water on solids and an aqueous polymer dispersion binder.

[0062] Flat elements were formed from the mixture and allowed to dry at room temperature for about 24 hours. The necessary dimensions are cut by a high pressure water jet cutter to form elements for the side walls and bottom of the crucible. The components are held together by using the example slurry. The green body is heated to about 600°C for 6 hours, then the temperature is slowly increased to about 1050°C until the pressure in the kiln drops. A nitrogen atmosphere of about 500 mbar was used during the firing process. During the next 4 days, the temperature was slowly increased to 1250°C during further heating, and finally, up to 1400°C. The crucible was then maintained at a temperature of 1400°C for the remainin...

example 2

[0064] Metal silicon powder with a particle size of less than 45 microns is mixed with 20% by weight of SiC powder with a particle size of less than 100 microns and a particle size of less than 10 microns (weight ratio 1:3). Water was added at 25% solids weight and the mixture was filled into molds, which were the outer surface of the crucible. The inner surface is formed by pressing a plunger into the material. After drying at room temperature for 30 minutes, the green body can be removed from the mold and plunger and fired according to the conditions of Example 1.

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PUM

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Abstract

A method for the manufacture of a crucible for the crystallization of silicon comprising the steps of preparing a slurry of a solid and a liquid consisting of metallic silicon powder, up to 25% by weight of SiC powder, up to 10% by weight of SiN, Composition of up to 0.5% by weight of catalyst, up to 1% by weight of binder; forming a green body of a crucible from the slurry; heating the green body in an atmosphere of nitrogen, optionally including an inert gas, so that silicon is at least partially bonded to silicon nitride reaction.

Description

technical field [0001] The invention relates to a method for producing a crucible for silicon ingot production and to the crucible. Background technique [0002] Silicon is an element with various industrial uses. [0003] One use is in photovoltaic applications. For the photovoltaic industry, ultrapure silicon is required. [0004] Photovoltaic solar energy is undergoing tremendous industrial development due to considerations related to climate change and energy supply. Reducing the cost of solar energy is critical to being competitive with conventional energy sources. [0005] For the production of solar cells, polycrystalline and monocrystalline silicon are used. Crystallization of silicon (silicon) or silicon (silicium, the old name of silicon) is generally performed by crystallization in a crucible. The method is based on the effect that silicon ingots can be produced from molten silicon by slow cooling. It is a method of directional solidification. It produces s...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C30B35/00C04B35/591F27B14/10
CPCC04B35/591C04B2235/3272C04B2235/3826C04B2235/428C04B2235/46C04B2235/5436C04B2235/5472C04B2235/656C04B2235/6562C04B2235/6567C04B2235/77C30B29/06C30B11/002Y10T117/1024C30B13/14C30B35/00C30B28/06
Inventor 鲁内·罗利格海泰
Owner STEULER SOLAR