Chitosan biological film-forming glue and preparation method thereof
A technology of chitosan and film-forming glue, which is applied in medical science, bandages, absorbent pads, etc., can solve the problems of limited application and poor solubility of chitosan, and achieves application promotion, high solubility and good biocompatibility. Effect
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[0065] Example 1
[0066] A chitosan biofilm forming glue, including the following raw materials in weight percentage:
[0067] Modified chitosan 0.5%
[0068] Mint 0.01%
[0069] Acidifier 0.05%
[0070] Scutellaria 0.2%
[0071] Cork 0.1%
[0072] Deionized water balance.
[0073] The modified chitosan is chitosan hydrochloride with a degree of deacetylation of 70%.
[0074] The acidulant is lactic acid with a relative density of 1.20 and a lactic acid anhydride content of 5%.
[0075] A preparation method of chitosan biofilm-forming glue includes the following steps:
[0076] A. Add 1 / 2 of the total amount of deionized water to the container, add the modified chitosan in the above proportion under stirring, and stir until it is completely dissolved;
[0077] B. Add the modified chitosan and other raw materials other than the acidulant in the above proportion under stirring, continue to stir for 5 minutes and then vacuum filter to obtain the filter residue and filtrate;
[0078] C. Add the re...
Example Embodiment
[0081] Example 2
[0082] A chitosan biofilm forming glue, including the following raw materials in weight percentage:
[0083] Modified chitosan 2.5%
[0084] Mint 0.04%
[0085] Acidifier 0.08%
[0086] Scutellaria 0.25%
[0087] Cork 0.15%
[0088] Deionized water balance.
[0089] The modified chitosan is carboxymethyl chitosan with a degree of carboxylation of 90%.
[0090] The acidulant is lactic acid with a relative density of 1.21 and a lactic acid anhydride content of 10%.
[0091] A preparation method of chitosan biofilm-forming glue includes the following steps:
[0092] A. Add 2 / 3 of the total amount of deionized water to the container, add the modified chitosan in the above proportion under stirring, and stir until completely dissolved;
[0093] B. Add the modified chitosan and other raw materials other than the acidulant in the above proportion under stirring, continue stirring for 6 minutes, and then vacuum filter to obtain filter residue and filtrate;
[0094] C. Add the remaini...
Example Embodiment
[0097] Example 3
[0098] A chitosan biofilm forming glue, including the following raw materials in weight percentage:
[0099] Modified chitosan 3%
[0100] Mint 0.08%
[0101] Acidifier 0.1%
[0102] Scutellaria 0.3%
[0103] Cork 0.2%
[0104] Deionized water balance.
[0105] The modified chitosan is a mixture of chitosan hydrochloride with a degree of deacetylation of 80% and carboxymethyl chitosan with a degree of carboxylation of 85%. The weight ratio of chitosan is 2.5:1.
[0106] The acidulant is lactic acid with a relative density of 1.22 and a lactic acid anhydride content of 15%.
[0107] A preparation method of chitosan biofilm-forming glue includes the following steps:
[0108] A. Add 1 / 2 of the total amount of deionized water to the container, add the modified chitosan in the above proportion under stirring, and stir until it is completely dissolved;
[0109] B. Add the modified chitosan and other raw materials other than the acidulant in the above proportion under stirring, co...
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