Salt for dye
A technology of dyes and substituents, applied in the field of salts for dyes, to achieve the effect of excellent solubility
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[0152] Hereinafter, the colored photosensitive resin composition of the present invention will be further described in detail through examples. "%" and "part" in an example refer to mass % and a mass part, unless otherwise indicated.
Synthetic example 1
[0154] 13 parts of methanol were added to 1.30 parts of lithium hydroxide monohydrate (manufactured by Wako Pure Chemical Industries, Ltd.), and stirred at 60 degrees. Further, a solution of 1.92 parts of boric acid (manufactured by Wako Pure Chemical Industries, Ltd.) and 11.55 parts of 2,2'-biphenol (manufactured by Tokyo Chemical Industry Co., Ltd.) dissolved in 67 parts of methanol was added and stirred at 60°C 7 hours. After cooling the mixed solution to room temperature, the precipitate was obtained by suction filtration and washed with 70 parts of acetone to obtain 5.62 parts of a compound represented by the formula (BC-26-Li).
[0155]
Synthetic example 2
[0157] 100 parts of methanol were added and dissolved in 2.00 parts of sodium hydroxide (manufactured by Wako Pure Chemical Industries, Ltd.). Further, 16.02 parts of 2,3-dihydroxynaphthalene (manufactured by Tokyo Chemical Industry Co., Ltd.) and 3.09 parts of boric acid (manufactured by Wako Pure Chemical Industries Co., Ltd.) were added, stirred at room temperature for two hours, and further stirred at 65 degrees 8 hours. After cooling the mixed solution to room temperature, the precipitate was obtained by suction filtration, washed with 268 parts of ion-exchanged water, 331 parts of methanol, and 869 parts of acetonitrile to obtain 4.16 parts of a compound represented by the formula (BC-25-Na).
[0158]
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