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Preparation method of iron oxide water-based color paste

A water-based color paste, iron oxide technology, applied in the direction of pigment paste, etc., can solve the problems of large specific gravity, unsuitable grinding and dispersion, coarse particles of water-based color paste, poor tinting strength, etc., to improve the dispersion performance, improve production efficiency and hiding power. strong effect

Active Publication Date: 2014-03-26
SHANGHAI BAIYAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the high molecular hardness of iron oxide pigment dry powder, it is not suitable for grinding and dispersing due to its large specificity. Therefore, the produced iron oxide pigment water-based color paste has coarse particles, 15-20 microns, easy to precipitate, and poor coloring power.

Method used

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  • Preparation method of iron oxide water-based color paste

Examples

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Comparison scheme
Effect test

Embodiment 1

[0020] (1) Use undried iron oxide pigments, also known as filter cakes. The parts by weight of water are 35, the filter cake is stirred, and the temperature is raised to 65°C.

[0021] (2) Add dropwise the alkyl polyoxyethylene ether as an anionic active agent and the branched chain alkyl alcohol ether phosphate salt as a high-performance dispersant, keep the temperature at 65°C, and keep stirring at a stirring speed of 1200 rpm ; The number of parts by weight of the alkyl polyoxyethylene ether is 3, and the number of parts by weight of the branched chain alkyl alcohol ether phosphate salt is 4; the slow dropwise addition is completed within 50 minutes.

[0022] (3) Add branched alcohol ether as a supplementary wetting agent, keep the temperature at 65° C., and keep stirring for 80 minutes; the weight part of branched alcohol ether is 2.

[0023] (4) After bubbles appear, cool down to room temperature; keep stirring.

[0024] (5) Add polyester-modified silicone oil as a defo...

Embodiment 2

[0028] (1) Use undried iron oxide pigments, also known as filter cakes. The parts by weight of water are 45, the filter cake is stirred, and the temperature is raised to 75°C.

[0029] (2) Add dropwise the alkyl polyoxyethylene ether as an anionic active agent and the branched chain alkyl alcohol ether phosphate salt as a high-performance dispersant, keep the temperature at 75°C, and keep stirring at a stirring speed of 1300 rpm ; The number of parts by weight of the alkyl polyoxyethylene ether is 6, and the number of parts by weight of the branched chain alkyl alcohol ether phosphate salt is 8; the slow dropwise addition is completed within 70 minutes.

[0030] (3) Add branched chain alcohol ether as a supplementary wetting agent, keep the temperature at 75° C., and keep stirring for 100 minutes; the weight part of branched chain alcohol ether is 3.

[0031] (4) After bubbles appear, cool down to room temperature; keep stirring.

[0032] (5) Add polyester-modified silicone ...

Embodiment 3

[0036] (1) Use undried iron oxide pigments, also known as filter cakes. The parts by weight of water are 40, the filter cake is stirred, and the temperature is raised to 70°C.

[0037] (2) Add dropwise the alkyl polyoxyethylene ether as an anionic active agent and the branched chain alkyl alcohol ether phosphate salt as a high-performance dispersant, keep the temperature at 70°C, and keep stirring at a stirring speed of 1300 rpm ; The number of parts by weight of the alkyl polyoxyethylene ether is 4, and the number of parts by weight of the branched chain alkyl alcohol ether phosphate salt is 6; the slow dropwise addition is completed within 60 minutes.

[0038] (3) Add branched chain alcohol ether as a supplementary wetting agent, keep the temperature at 70° C., and keep stirring for 90 minutes; the weight part of branched chain alcohol ether is 2.5.

[0039] (4) After bubbles appear, cool down to room temperature; keep stirring.

[0040] (5) Add polyester-modified silicone...

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Abstract

The invention relates to a preparation method of an iron oxide water-based color paste, which comprises the following steps: (1) stirring undried iron oxide pigment, and heating to 65-75 DEG C; (2) dropwisely adding 3-6 parts by weight of anionic active agent and 4-8 parts by weight of high-performance dispersing agent, keeping the temperature at 65-75 DEG C, and continuously stirring; (3) adding 2-3 parts by weight of supplementary wetting agent, keeping the temperature at 65-75 DEG C, and continuously stirring; (4) after bubbles appear, cooling to room temperature; (5) adding 0.3-0.5 part by weight of defoaming agent; and (6) adding deionized water to obtain the iron oxide water-based color paste. According to the invention, the prepared iron oxide pigment has high dispersity, fine granularity and strong coloring power.

Description

technical field [0001] The invention relates to the field of pigments, in particular to a preparation method of iron oxide water-based color paste. technical background [0002] Water-based color paste has a wide range of uses. It only needs to directly add water-based color paste to the prepared base material to efficiently produce various colors of coatings, inks and textile printing materials. Widely used in coatings, leather, printing, paper making, latex, textile and other industries. [0003] The iron oxide series pigment water-based color paste currently produced and sold on the market is made of iron oxide pigment dry powder by adding additives and water using a physical colloidal grinding process, that is, sanding with a sander for multiple times. Due to the high molecular hardness of iron oxide pigment dry powder, it is not suitable for grinding and dispersing due to its large specificity. Therefore, the produced iron oxide pigment water-based color paste has coar...

Claims

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Application Information

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IPC IPC(8): C09D17/00
Inventor 蒋加寿周定兴
Owner SHANGHAI BAIYAN IND
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