A kind of anti-shrinkage antibacterial finishing agent and preparation method thereof
A finishing agent and anti-shrinkage technology, which is applied in fiber treatment, plant fiber, textiles and papermaking, etc. It can solve the problems of shrinkage of clothes and the lack of antibacterial properties of ordinary clothes
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Embodiment 1
[0009] (1) Adjust the temperature of the vacuum reactor to 75°C, and maintain the vacuum state in the reactor; (2) Put 40kg of 1,3-propanediol, 180kg of water, dodecyl poly 12kg of ethylene glycol ether, 3kg of ethylene glycol diglycidyl ether, and stir evenly with the stirring paddle that comes with the vacuum reactor; (3) Add 3kg of zeolite powder, 4kg of gelatin, and tea through the feeding window of the vacuum reactor again. The content of polyphenol is 2kg, potassium metaphosphate is 6kg, and it is stirred for 30 minutes under vacuum; (4) After stirring evenly, the reaction kettle is restored to normal pressure, and the finishing solution is homogenized with a homogenizing pump. The homogenizing pressure is 25Mpa, and the homogenizing time is 10 minutes; (5) After homogenization, seal the finishing agent and store it at low temperature.
Embodiment 2
[0011] (1) Adjust the temperature of the vacuum reactor to 73°C, and maintain the vacuum state in the reactor; (2) Put 50kg of 1,3-propanediol, 200kg of water, dodecyl poly Ethylene glycol ether is 8kg, ethylene glycol diglycidyl ether is 4kg, and stirred evenly with the stirring paddle that comes with the vacuum reactor; (3) Add 4kg of zeolite powder, 3kg of gelatin, and tea through the feeding window of the vacuum reactor again. 3kg of polyphenols, 2kg of potassium metaphosphate, stirring for 30min in a vacuum state; (4) After stirring evenly, return the reactor to normal pressure, and homogenize the finishing solution with a homogenizing pump. The homogenizing pressure is 20Mpa, and the homogenizing time 7 minutes; (5) After homogenization, seal the finishing agent and store it at low temperature.
Embodiment 3
[0013] (1) Adjust the temperature of the vacuum reactor to 70°C, and maintain the vacuum state in the reactor; (2) Put 60kg of 1,3-propanediol, 190kg of water, and dodecylpolyethylene into the vacuum reactor through the feeding window. 10kg of ethylene glycol ether, 6kg of ethylene glycol diglycidyl ether, and stir evenly with the stirring paddle that comes with the vacuum reactor; (3) Add 5kg of zeolite powder, 3kg of gelatin, and tea through the feeding window of the vacuum reactor again. 2kg of polyphenols, 4kg of potassium metaphosphate, stirring for 30min in a vacuum state; (4) After stirring evenly, return the reactor to normal pressure, homogenize the finishing solution with a homogenizing pump, the homogenizing pressure is 25Mpa, and the homogenizing time 5 minutes; (5) After homogenization, seal the finishing agent and store it at low temperature.
[0014] Soak the pure cotton coat in the finishing agent of Example 1, Example 2, and Example 3 at room temperature for 4...
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