liquid ink
A technology of ink and liquid, applied in the direction of ink, application, coating, etc., can solve the problems of large volume, difficult connector connection, etc., achieve the effect of simple process, maintain rigidity, and achieve reflow resistance
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Embodiment 1
[0079] Dissolve 7 g of N-phenyl-3-aminopropyltrimethoxysilane (KBM573, trade name manufactured by Shin-Etsu Silicone Co., Ltd.) as a surface treatment agent in 300 g of methyl ethyl ketone, and add 700 g thereof while stirring as Silica F05-12 (trade name, manufactured by Fukushima Ceramics Co., Ltd.) was crushed, followed by further stirring at room temperature for 1 hour. Agglomerated components of the crushed silica were filtered through a 200-mesh nylon cloth to obtain a slurry-like filtrate (silica slurry). 350g of a copolymer of glycidyl methacrylate, ethyl acrylate and butyl acrylate (weight average molecular weight 1.3 million, epoxy equivalent 7800, Tg-45°C) as an acrylic resin in methyl ethyl ketone (MEK) solution (concentration: 20% by mass), 34.2g of MEK solution (concentration: 50% by mass) of biphenyl aralkyl type epoxy resin (NC-3000H, trade name manufactured by Nippon Kayaku Co., Ltd.), 25.8g of phenolic resin (LA-3018 , Dainippon Ink Co., Ltd. product name) M...
Embodiment 2~11
[0080] Examples 2-11, Reference Examples 1-4 and Comparative Examples 5-8
[0081] A liquid ink was prepared in the same manner as in Example 1, except that each material shown in Tables 1 and 2 was used in the compounding ratio shown in the table. The mixing ratio of organic polymer, thermosetting resin and curing agent is based on the mass of the thermosetting resin composition except for the inorganic filler, and the mixing ratio of the inorganic filler is based on the total solid content of the thermosetting resin composition (in liquid ink Components other than the solvent) are based on the mass of the compounding ratio.
Embodiment 12
[0083] Dissolve 7 g of N-phenyl-3-aminopropyltrimethoxysilane (KBM573, product name manufactured by Shin-Etsu Silicone Co., Ltd.) as a surface treatment agent in 300 g of cyclohexanone, and add 700 g of it as a spherical dimethicone while stirring. Silica SO-25R (trade name manufactured by Admatechs Co., Ltd.) was further stirred at room temperature for 1 hour. Agglomerated components of the spherical silica were filtered using a 200-mesh nylon cloth to obtain a slurry-like filtrate (silica slurry). 350 g of a cyclohexanone solution (concentration 20% by mass) of a copolymer of glycidyl methacrylate, acrylonitrile, ethyl acrylate, and butyl acrylate (weight average molecular weight: 450,000, Tg-14.7°C) as an acrylic resin, 34.2 g of cyclohexanone solution (concentration: 50% by mass) of biphenyl aralkyl type epoxy resin (NC-3000H, trade name manufactured by Nippon Kayaku Co., Ltd.), 25.8 g of phenolic resin (LA-3018, Dainippon Ink Co., Ltd. propylene glycol monomethyl ether s...
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Abstract
Description
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