A discoloration agent for textile fabrics
A technology of textile fabrics and color-changing agents, applied in the field of functional dyes, can solve the problems of complex preparation methods and limited color-changing dye systems, and achieve the effects of enhanced light reflection, excellent reversible thermochromic properties, and strong adhesion
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preparation example 1
[0050] Take 1mol of 2-(4'-diethylamino-2'-hydroxybenzoyl)-benzoic acid and 1mol of 2-diethylamino-4-hydroxyl-6-methyl-pyrimidine in the presence of 10mol of acetic anhydride under reflux for 4 hours, cooled, the reactant was poured into ice water, neutralized with sodium hydroxide to produce a precipitate, filtered, washed with water, dried to obtain a crude product, then recrystallized in cyclohexane, and decolorized with activated carbon, The target product A1 was obtained with a yield of 95.4% and a melting point of 176-177°C.
[0051]
preparation example 2
[0053] In addition to replacing 2-diethylamino-4-hydroxyl-6-methyl-pyrimidine with 2-dimethylamino-4-hydroxyl-6-methyl-pyrimidine, it was prepared in the same manner as in Preparation Example 1 Example 2, to obtain compound A2 with a yield of 97.2% and a melting point of 182-183.5°C.
[0054]
preparation example 3
[0056] Divide by 2-(4'-dimethylamino-2'-hydroxybenzoyl)-benzoic acid replacing 2-(4'-diethylamino-2'-hydroxybenzoyl)-benzoic acid and divide by 2 -Dimethylamino-4-hydroxyl-6-methyl-pyrimidine replaced 2-diethylamino-4-hydroxyl-6-methyl-pyrimidine, and Preparation Example 3 was carried out in the same manner as Preparation Example 1, Compound A3 was obtained with a yield of 96.7% and a melting point of 179-180.4°C.
[0057]
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