Treatment method for jointly performing oxidation of trivalent arsenic and reduction of hexavalent chromium by using organic acid
A treatment method and technology of trivalent oxidation, applied in the direction of reducing water/sewage treatment, oxidized water/sewage treatment, chemical instruments and methods, etc.
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Embodiment 1
[0029] 100 mL of a mixed solution of 2 mM oxalic acid in water with an As(III) concentration of 1 mM and a Cr(VI) concentration of 0.6 mM, and adjusting the pH value to 3 with sulfuric acid;
[0030] One is 100mL of a mixed solution of As(III) concentration of 1mM and oxalic acid 2mM, and the pH value is adjusted to 3 by sulfuric acid; the other is 100mL of a mixed solution of Cr(VI) concentration of 0.6mM and oxalic acid 2mM, and the pH value is adjusted by sulfuric acid. Adjust the pH value to 3; one is 100 mL of a mixed solution with a concentration of As(III) of 1 mM and a concentration of Cr(VI) of 0.6 mM, and adjust the pH value to 3 with sulfuric acid.
[0031] Such as figure 1 and figure 2 As shown, the reaction can only proceed when As(III), Cr(VI) and oxalic acid coexist, and the treatment efficiency is high. No reaction occurs when any other two substances coexist.
Embodiment 2
[0033] 100 mL of a mixed solution of 4 mM citric acid in water with an As(III) concentration of 1 mM and a Cr(VI) concentration of 1.2 mM, and adjusting the pH value to 2 with sulfuric acid;
[0034] Such as image 3 As shown, citric acid with a dicarboxylic structure can also make As(III) and Cr(VI) have a synergistic redox effect.
Embodiment 3
[0036] Add 5 mM oxalic acid in water with As(III) concentration of 1 mM and Cr(VI) concentration of 3 mM, and adjust the pH value to 2 with sulfuric acid.
[0037] Such as Figure 4 As shown, the greater the amount of oxalic acid, the lower the pH value, the more favorable the redox of arsenic and chromium.
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