A composite impregnating agent capable of improving the service life of metallized film capacitors and its preparation method
A metallized film and composite technology, applied in capacitors, fixed capacitors, drying/impregnating machines, etc., can solve the problems of high dielectric loss, poor thermal stability, and secondary moisture of oil to achieve low dielectric loss and thermal expansion coefficient, which is beneficial to the life of the capacitor and prevents the effect of secondary moisture
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Embodiment 1
[0028] (1) Preparation of modified soybean oil:
[0029] a) Put ordinary soybean oil in a reaction kettle, add hydrogen peroxide, glacial acetic acid and 98% concentrated sulfuric acid in sequence, and heat and stir at 45°C for 6 hours; among them, soybean oil, hydrogen peroxide, glacial acetic acid and concentrated The mass ratio of sulfuric acid is: 6.0 parts of soybean oil, 3.5 parts of 15% hydrogen peroxide, 2.0 parts of glacial acetic acid, and 0.6 parts of 98% concentrated sulfuric acid;
[0030] b) Leave the soybean oil after the complete stirring reaction for 2 hours, and monitor in real time through the sight glass on the reactor until the soybean oil in the reactor is completely separated; Discharge, the supernatant liquid that stays in the reactor is modified soybean oil;
[0031] (2) Preparation of modified molecular sieves:
[0032] a) Put conventional molecular sieves into a high-speed stirring tank, heat and stir at a speed of 4800 rpm for 3 hours until crushe...
Embodiment 2
[0040] (1) Preparation of modified soybean oil:
[0041] a) Put ordinary soybean oil in a reaction kettle, add hydrogen peroxide, glacial acetic acid and 98% concentrated sulfuric acid in sequence, and heat and stir at 40°C for 6 hours; among them, soybean oil, hydrogen peroxide, glacial acetic acid and concentrated The mass ratio of sulfuric acid is: 7.0 parts of soybean oil, 3.5 parts of 15% hydrogen peroxide, 1.5 parts of glacial acetic acid, and 1.0 part of 98% concentrated sulfuric acid;
[0042] b) The soybean oil after the complete stirring reaction was left to stand for 1 hour, and the real-time monitoring was carried out through the sight glass on the reactor until the soybean oil in the reactor was completely separated; Discharge, the supernatant liquid that stays in the reactor is modified soybean oil;
[0043] (2) Preparation of modified molecular sieves:
[0044] a) Put conventional molecular sieves into a high-speed stirring tank, heat and stir at a speed of 4200...
Embodiment 3
[0052] (1) Preparation of modified soybean oil:
[0053] a) Put ordinary soybean oil in a reaction kettle, add hydrogen peroxide, glacial acetic acid and 98% concentrated sulfuric acid in sequence, and heat and stir at 50°C for 5 hours; among them, soybean oil, hydrogen peroxide, glacial acetic acid and concentrated The mass ratio of sulfuric acid is: 5.5 parts of soybean oil, 4.5 parts of 10% hydrogen peroxide, 2.5 parts of glacial acetic acid, and 0.5 part of 98% concentrated sulfuric acid;
[0054] b) The soybean oil after the complete stirring reaction was left to stand for 1 hour, and the real-time monitoring was carried out through the sight glass on the reactor until the soybean oil in the reactor was completely separated; Discharge, the supernatant liquid that stays in the reactor is modified soybean oil;
[0055] (2) Preparation of modified molecular sieves:
[0056] a) Put conventional molecular sieves into a high-speed stirring tank, heat and stir at a speed of 55...
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