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Medicament foil rolling additive composition

A technology of additives and compositions, applied in the directions of additives, lubricating compositions, petroleum industry, etc., can solve the problem of the decrease of peeling strength and dyne value of medicated foil, extremely low requirement of residual amount on the surface of medicated foil, and low dyne value and peeling strength and other problems, to achieve the effect of improving the dyne value and peeling strength of the drug foil, reducing the residual amount on the surface of the drug foil product, and reducing the residual amount on the surface.

Active Publication Date: 2014-08-13
石家庄新泰特种油有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Since the medicinal foil product is delivered in a hard state, without annealing and degreasing process, it is required that the additives can meet the lubrication requirements of double-sheet foil rolling, and at the same time, the residue on the surface of the medicinal foil after rolling is extremely low. In order to ensure For rolling lubrication, additives generally improve the lubricating ability through chemical adsorption and high carbon chain composition. For example, C12-C16 saturated fatty alcohol and C12-C16 fatty acid methyl ester are used as the main additives. The wetting property is too strong, and at the same time, the C12-16 saturated fatty acid methyl ester has insufficient cleaning ability on the surface of the medicinal foil, resulting in a decrease in the peel strength and dyne value of the medicinal foil. At present, the dyne value of the medicinal foil in my country is required to be no less than 34. The strength requirement is not less than 8, and the existing technology generally has low dyne value and peel strength

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Take raw materials according to the following weight ratio:

[0025] (A) Low-temperature antioxidant: 2,6-di-tert-butyl-p-cresol, 0.04%;

[0026] (B) Fatty acid methyl ester: C14 fatty acid methyl ester, 85%;

[0027] (C) Phosphide antiwear agent: phosphate ester amine salt, 0.06%;

[0028] (D) Polyhydric alcohol: Trimethylolpropane, 13.9%;

[0029] (E) High temperature antioxidant: p, p-diisooctyl diphenylamine, 1.0%;

[0030] Mix the above components in proportion, and stir at 50-80° C. for 1 hour until they are completely dissolved and form a transparent liquid, thus obtaining the composition of the present invention.

Embodiment 2

[0032] Take raw materials according to the following weight ratio:

[0033] (A) Low temperature antioxidant: 2,6-di-tert-butyl-p-cresol, 1.0%; 4,4-methylene bis-2,6-di-tert-butyl-p-cresol, 1.0%;

[0034] (B) Fatty acid methyl ester: C14 fatty acid methyl ester, 30%; C12 fatty acid methyl ester, 50%;

[0035] (C) Phosphide antiwear agent: triaryl phosphate, 0.3%; tricresyl phosphate, 0.7%;

[0036] (D) Polyhydric alcohol: pentaerythritol, 15%;

[0037] (E) High temperature antioxidant: octylbutyldiphenylamine, 2.0%;

[0038] Mix the above components in proportion, and stir at 50-80° C. for 1 hour until they are completely dissolved and form a transparent liquid, thus obtaining the composition of the present invention.

Embodiment 3

[0040] Take raw materials according to the following weight ratio:

[0041] (A) Low-temperature antioxidant: 4,4-methylenebis-2,6-di-tert-butyl-p-cresol, 0.06%;

[0042] (B) Fatty acid methyl ester: C14 fatty acid methyl ester, 90%;

[0043] (C) Phosphide antiwear agent: tricresyl phosphate, 0.2%; phosphate amine salt, 0.7%;

[0044] (D) Polyhydric alcohols: pentaerythritol, 4%; diethylene glycol, 5%;

[0045] (E) High temperature antioxidant: octylbutyldiphenylamine, 0.04%;

[0046] Mix the above components in proportion, and stir at 50-80° C. for 1 hour until they are completely dissolved and form a transparent liquid, thus obtaining the composition of the present invention.

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PUM

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Abstract

The invention discloses a medicament foil rolling additive composition. The composition consists of the following components by weight: (A) 0.04-2.0% of low-temperature antioxidant, (B) 80-95% of fatty acid methyl ester, (C) 0.06-1.0% of phosphide anti-wear agent, (D) 1-15% of polyhydric alcohol and (E) 0.04-2.0% of high-temperature antioxidant, wherein the component (C) phosphide anti-wear agent is one or more of triaryl phosphate, tricresyl phosphate and phosphate amine salt; the component (D) polyhydric alcohol is one or more of trimethylolpropane, pentaerythritol and diethylene glycol. By compounding the carbon chain fatty acid methyl ester, the phosphide anti-wear agent and the polyhydric alcohol, the chemical adsorption capability and the flow cleaning performance are enhanced, the surface residue of a medicament foil product is greatly reduced on the premise of ensuring the lubricating capability, and the dyne value and peeling strength of a medicament foil are effectively improved.

Description

technical field [0001] The present invention relates to a medicinal foil rolling additive composition. Background technique [0002] During the rolling process, it is necessary not only to meet the rolling lubrication requirements, but also to meet the purpose of degreasing the aluminum foil after rolling without annealing. The cleanliness of degreasing directly determines the dyne value and peel strength of the foil. [0003] Since the medicinal foil product is delivered in a hard state, without annealing and degreasing process, it is required that the additives can meet the lubrication requirements of double-sheet foil rolling, and at the same time, the residue on the surface of the medicinal foil after rolling is extremely low. In order to ensure For rolling lubrication, additives generally improve the lubricating ability through chemical adsorption and high carbon chain composition. For example, C12-C16 saturated fatty alcohol and C12-C16 fatty acid methyl ester are used ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M141/10C10M169/04C10N40/24C10N30/04C10N30/06
Inventor 丁峰丁浩李学兵周志刚张慧财刘想孙彦松田鑫
Owner 石家庄新泰特种油有限公司
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