Spice for costustoot flavored cigarettes based on aquilaria leaves, as well as preparation method and application of spice

A kind of agarwood leaf and wood incense technology, applied in the directions of essential oils/spice, application, tobacco, etc., can solve the problems of low overall utilization rate of white wood incense resources, difficult to obtain economic benefits, etc., achieve good economic and social benefits, increase alcohol and degree, improve the effect of taste absorption

Active Publication Date: 2014-08-27
SHENZHEN TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In recent years, in order to meet the growing demand for agarwood from the society, white wood incense trees have begun to be widely planted in China. The white wood incense trees produce fragrance in the trunks. The overall utilization rate of incense resources is low, and it is difficult to obtain obvious economi

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Grind the leaves of A. chinensis through a 40-mesh sieve, add distilled water 4 times the weight of the powder of A. chinensis and 0.7% of a compound enzyme relative to the weight of the powder of A. chinensis, that is, β-glucanase 3.5 million U / mL, Cellulase 150,000 U / mL, hemicellulase 1.5 million U / mL, pectinase 10,000 U / mL, the volume ratio of the four enzymes is 1:3:2:1,

[0024] 40 °C water bath constant temperature treatment for 3 h. Add ethanol until the total solvent is 8 times the mass of Akiras sinensis leaf powder, heat reflux at 70°C for 1.5h, and extract 3 times, combine the extracts and then concentrate under reduced pressure to the state of extract, place the extract in supercritical CO 2 In the extraction kettle, add 100% ethanol with a concentration of 0.7 times of the weight of the raw material of Akira sinensis leaf powder, set the extraction pressure of the extraction kettle to 22 MPa, the extraction temperature to 45 ° C, the extraction time to 3 ho...

Embodiment 2

[0028] Grind the leaves of A. chinensis through a 60-mesh sieve, add distilled water 6 times the weight of the powder of A. chinensis and 0.3% of a compound enzyme relative to the weight of the powder of A. chinensis, that is, β-glucanase 3.5 million U / mL, Cellulase 150,000 U / mL, hemicellulase 1.5 million U / mL, pectinase 10,000 U / mL, the volume ratio of the four enzymes is 1:2:2:1,

[0029] 60 °C water bath constant temperature treatment for 1 h. Add ethanol until the total solvent is 10 times the mass of Akiras sinensis leaf powder, heat reflux at 90°C for 0.5 h, and the extraction frequency is 1 time, combine the extracts and then concentrate under reduced pressure to the state of extract, and place the extract in supercritical CO 2 In the extraction kettle, add 90% ethanol with a concentration of 0.3 times of the weight of the raw material of Akira sinensis leaf powder, set the extraction pressure of the extraction kettle to 28 MPa, the extraction temperature to 50°C, the e...

Embodiment 3

[0033] Grind the leaves of A. chinensis through a 50-mesh sieve, add distilled water 5 times the weight of the powder of A. chinensis and 0.5% of a compound enzyme relative to the weight of the powder of A. chinensis, that is, β-glucanase 3.5 million U / mL, Cellulase 150,000 U / mL, hemicellulase 1.5 million U / mL, pectinase 10,000 U / mL, the volume ratio of the four enzymes is 1:2:2:2,

[0034] 50 °C water bath constant temperature treatment for 2 h. Add ethanol until the total solvent is 9 times the mass of Akiras sinensis leaf powder, heat reflux at 80°C for 1 h, and extract twice, combine the extracts and then concentrate under reduced pressure to the state of extract, and place the extract in supercritical CO 2 In the extraction kettle, add 95% ethanol with a concentration of 0.5 times the weight of the raw material of Akira sinensis leaf powder, set the extraction pressure of the extraction kettle to 25 MPa, the extraction temperature to 47 °C, the extraction time to 2.5 h, C...

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PUM

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Abstract

The invention provides a method for preparing spice of costustoot flavored cigarettes based on aquilaria leaves. The method comprises the following steps: crushing and screening aquilaria leaves; performing enzyme treatment; performing heat reflux extraction; carrying out solid-liquid separation; concentrating at reduced pressure; performing supercritical CO2 extraction; reclaiming an entrained solvent; carrying out membrane separation, sectioning and dicing; and preparing to obtain the novel spice of the costustoot flavored cigarette based on aquilaria leaves. The spice has the characteristics that the aquilaria leaves with rich resources are used as a raw material, are subjected to wall-breaking treatment by using an enzyme method and are treated by heat reflux extraction to obtain an extract; aquilaria leaf essential oil is extracted from the extract by using a supercritical extraction process, and the extraction yield can be remarkably increased by virtue of the combined process; the aquilaria leaf essential oil is sectioned and diced by using membrane separation, and is mixed with guaiacol, santalol, cedar camphor, vetiver oil, ethanol and propylene glycol in a certain proportion; the prepared spice is added into cigarettes in a certain weight proportion. Therefore, the cigarettes are mellow and rich in flavor, the fragrance is improved, an elegant costustoot flavor is given to the cigarettes, and the sensing quality of the cigarettes can be remarkably improved.

Description

technical field [0001] The invention belongs to the technical field of flavoring essence for tobacco, and in particular relates to a novel woody flavor tobacco flavor based on agarwood leaves and its preparation method and application. Applying the woody flavor flavor to cigarettes can significantly improve the senses of cigarettes quality. Background technique [0002] Agarwood is the oil secreted by Daphneaceae plants in the process of self-repair after being damaged by nature or man-made, or the secretion condensed by fungal infection. It is a traditional precious medicinal material and natural spice. The only resource of agarwood is mainly distributed in Guangdong, Guangxi, Yunnan, Fujian, and Hainan. Due to the long cycle of wild agarwood and excessive logging and mining, wild agarwood is now on the verge of extinction. In recent years, in order to meet the growing demand for agarwood from the society, white wood incense trees have begun to be widely planted in China. ...

Claims

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Application Information

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IPC IPC(8): C11B9/02A24B15/30
Inventor 王加深吕乔畅晓渊刘晓晖尉朝陈必春陈长青文祖艺
Owner SHENZHEN TOBACCO IND
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