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Fiber neat paste test piece forming method for scanning microscope

A technology of scanning microscopy and forming method, which is applied in the field of microscopic testing, can solve the problem that it is difficult to guarantee the shape, size and surface smoothness of the test piece, it is difficult to ensure that the test piece can meet the experimental requirements, and the shape of the test piece can only be relatively simple, etc. problems, to achieve the effect of facilitating observation, saving manpower and material resources, and reducing energy consumption

Active Publication Date: 2014-08-27
YANGZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although this molding method guarantees the original growth environment of the specimen, since concrete is a brittle material and the size of the specimen required for the SEM experiment is small, the cutting process can easily cause damage to the material and waste of the specimen higher rate
Moreover, it is difficult to guarantee the shape, size and surface smoothness of the test piece when cutting the shaped test piece with a cutting machine, and the shape of the test piece can only be relatively simple.
Due to the limitation of the depth of field of the scanning electron microscope, it is difficult to ensure that the obtained specimens can meet the experimental requirements
When forming standard test pieces, it will also cause unnecessary material waste

Method used

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  • Fiber neat paste test piece forming method for scanning microscope
  • Fiber neat paste test piece forming method for scanning microscope
  • Fiber neat paste test piece forming method for scanning microscope

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] carved as figure 1 , 2 For the upper mold 1 and the bottom plate 2 shown, brush oil on the surface of the upper mold 1 and the bottom plate 2, weigh 500g of cement and 150ml of water and stir with the NJ-160A slurry mixer, set it to automatic mixing, and clean the slurry with cement after the mixing is completed Fill the groove 5 on the bottom plate 2, vibrate lightly 20 times, level it, repeat 2 times, place the basalt fiber 3 parallel to the surface of the filled groove 5 along the length direction of the test piece, place the mold 1 on Fix the bottom plate 2 and the upper mold 1 with the clamp 4 at the corresponding position on the base plate 2, and wait for half an hour to wait for the initial setting of the cement slurry; stir the cement slurry with the same mixing ratio again, and fill the through groove 8 of the upper mold 1 , gently vibrated 20 times, leveled, and repeated 2 times until the surface of the test piece was flat, removed the mold after 24 hours, an...

Embodiment 2

[0022] carved as figure 1 , 2 The upper mold 1 and the bottom plate 2 are brushed with oil on the surface, weighed 500g of cement and 148ml of water and stirred with an NJ-160A pure slurry mixer, set to automatic stirring, and filled the groove 5 on the bottom plate 2 with the clean slurry after the stirring is completed , gently vibrated 20 times, leveled, repeated 2 times, put the plastic steel fiber 3 parallel to the surface of the filled groove 5 along the length direction of the test piece, put the upper mold 1 on the corresponding position on the bottom plate 2, and use the clamp 4. Fix the bottom plate 2 and the upper mold 1, let it stand for half an hour, and wait for the initial setting of the cement slurry; stir the cement slurry with the same mix ratio again, fill the through groove 8 of the upper mold 1, and vibrate gently 20 times, Leveling, repeating 2 times until the surface of the test piece 7 is flat, remove the mold after 24 hours, take it out after 28 days ...

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Abstract

The invention belongs to the field of microscopic tests of micro nano mechanics and fiber concrete and mainly relates to a fiber neat paste test piece forming method for a scanning microscope. The fiber neat paste test piece forming method is mainly characterized by comprising the steps: engraving upper moulds and bottom plates in shapes of three test pieces by using a laser engraving machine; filling the grooves in the bottom plate by using cement neat paste successively, putting fibers in parallel on the surfaces of the filled grooves along the length directions of the grooves, correspondingly placing the upper moulds on the bottom plates, filling through grooves by using neat concrete paste, and curing for multiple days. The fiber neat paste test piece forming method is simple in process and safe in operation. The fiber neat paste test piece forming method has the beneficial effects that (1) shapes and sizes of test pieces can be automatically designed as required, and the characteristic of diversification is achieved; (2) the test pieces are formed without pouring standard test pieces, thus saving manpower and material resource and reducing energy consumption; (3) a test piece mould can be repeatedly used and is low in cost; and (4), the depth of the fibers is manually controlled, so that the scanning microscope is observed conveniently.

Description

technical field [0001] The invention belongs to the micro-test field of micro-nano mechanics and fiber concrete, and mainly relates to a method for forming a fiber-cleaned slurry test piece for scanning the micro-environment. Background technique [0002] Now, concrete research has gradually shifted from a simple macro performance test to a research method combining macro and micro tests. In the microscopic experiment of fiber-reinforced concrete, it is necessary to study the interaction mechanism between fiber and cement slurry, so as to analyze the contribution of fiber to concrete strength. In the existing microscopic test method, the standard test block is cut to obtain the size and shape required for the experiment. Although this molding method guarantees the original growth environment of the specimen, since concrete is a brittle material and the size of the specimen required for the SEM experiment is small, the cutting process can easily cause damage to the material ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/28
Inventor 杨鼎宜丁苏金
Owner YANGZHOU UNIV
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