Method for manufacturing low-cost three-dimensional-structure graphene-aluminum supercapacitor composite electrode material
A supercapacitor and three-dimensional structure technology, which is applied in the manufacture of hybrid/electric double layer capacitors, metal material coating technology, gaseous chemical plating, etc., can solve the problem of difficult to use graphene materials with high specific surface area and excellent electrical properties Problems such as the performance of olefin-based supercapacitors, low-density agglomeration and stacking of graphene materials can reduce the probability of electron annihilation, optimize the charge transport path, and improve the charge-discharge response rate.
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specific Embodiment approach 1
[0018] Specific embodiment one: the preparation method of a kind of low-cost three-dimensional structure graphene-aluminum supercapacitor composite electrode material described in this embodiment is specifically carried out according to the following steps:
[0019] 1. Place the base material in the plasma-enhanced chemical vapor deposition vacuum device, evacuate to a pressure below 5Pa, pass in argon gas, adjust the flow rate of the argon gas to 10sccm-40sccm, and adjust the plasma-enhanced chemical vapor deposition vacuum device The pressure is 100Pa~300Pa, and under the pressure of 100Pa~300Pa and argon atmosphere, the temperature is raised to 400℃~600℃ within 25min;
[0020] 2. Introduce methane gas, adjust the gas flow rate of methane to 5sccm~40sccm, adjust the gas flow rate of argon to 60sccm~95sccm, adjust the pressure in the plasma enhanced chemical vapor deposition vacuum device to 200Pa~700Pa, and then set the radio frequency power to 150W ~250W, the pressure is 20...
specific Embodiment approach 2
[0028] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the matrix material described in step 1 is a three-dimensional structure aluminum matrix material. Others are the same as in the first embodiment.
specific Embodiment approach 3
[0029] Embodiment 3: This embodiment differs from Embodiment 1 or Embodiment 2 in that: the aluminum matrix material with a three-dimensional structure is foamed aluminum, porous aluminum or surface-corroded aluminum. Others are the same as in the first or second embodiment.
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