Method for manufacturing immiscible alloy ingot casting in aluminothermic reduction-slag refining mode

An immiscible alloy and slag refining technology, which is applied in the field of metallurgy, can solve the problems of high inclusions in alloy ingots, large fluctuations in alloy composition, and many pore defects, and achieve oxygen content removal, raw material cost reduction, and simple operation Effect

Active Publication Date: 2014-10-29
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Zhang Ting'an, Dou Zhihe, etc. proposed in the patent application number 200510047309.7 to use oxides as raw materials to prepare large-size homogeneous copper-chromium alloy contact materials by aluminothermic reduction-electromagnetic casting method, and realized the production of large-size copper-chromium alloy contact materials. However, there are quality problems such as high inclusions and many porosity defects in the prepared alloy ingot
Zhang Ting'an et al., based on the technology disclosed in the patent applic

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0061] According to the composition of the immiscible alloy ingot to be prepared, three parts of metal oxide powder are respectively prepared, and the metal oxide powder is Cu-based metal oxide powder, which is composed of CuO powder and PbO powder;

[0062] Mix each part of metal oxide powder with Al powder respectively, then add slag-forming agent CaO, respectively, in each part, CaO accounts for 2%, 3% and 5% of the total weight of metal oxide powder and Al powder, and mix all the materials. After uniformity, three batches of materials to be reduced are made;

[0063] The mixing ratios of CuO powder, PbO powder and Al powder are respectively 100:4.5:28, 100:320:60 and 100:775:105 by weight when each part is mixed and batched;

[0064] Put the materials to be reduced into the reactor respectively, and put Mg powder on the surface of the materials to be reduced, ignite the Mg powder directly with an open flame, and initiate the aluminothermic reduction reaction. Three high-t...

Embodiment 2

[0072] According to the composition of the immiscible alloy ingot to be prepared, three parts of immiscible metal oxide powder are respectively prepared, and the metal oxide powder is Cu-based metal oxide powder, which is composed of CuO powder and CoO powder;

[0073] Mix each part of metal oxide powder with Al powder respectively, then add slag-forming agent CaO, respectively, in each part, CaO accounts for 2%, 3% and 5% of the total weight of metal oxide powder and Al powder, and mix all the materials. After uniformity, three batches of materials to be reduced are made;

[0074] The mixing ratios of CuO powder, CoO powder and Al powder are respectively 100:6:30, 100:150:90 and 100:350:175 by weight when each part is mixed and batched;

[0075] Put the materials to be reduced into the reactor respectively, and put Mg powder on the surface of the materials to be reduced, ignite the Mg powder directly with an open flame, and initiate the aluminothermic reduction reaction. Thr...

Embodiment 3

[0083] According to the composition of the immiscible alloy ingot to be prepared, three parts of metal oxide powder are prepared respectively. The metal oxide powder is Cu-based metal oxide powder, which is composed of CuO powder and Fe 2 O 3 powder composition;

[0084] Mix each part of metal oxide powder with Al powder respectively, then add slag-forming agent CaO, respectively, in each part, CaO accounts for 2%, 3% and 5% of the total weight of metal oxide powder and Al powder, and mix all the materials. After uniformity, three batches of materials to be reduced are made;

[0085]CuO powder, Fe 2 O 3 The mixing ratios of powder and Al powder are respectively 100:5.5:30, 100:50:48 and 100:115:75 by weight;

[0086] Put the materials to be reduced into the reactor respectively, and put Mg powder on the surface of the materials to be reduced, ignite the Mg powder directly with an open flame, and initiate the aluminothermic reduction reaction. Three high-temperature melts ...

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Abstract

The invention discloses a method for manufacturing an immiscible alloy ingot casting in an aluminothermic reduction-slag refining mode, and belongs to the technical field of metallurgy. The method comprises the following steps that (1) according to components of the immiscible alloy ingot casting to be manufactured, metallic oxide powder is prepared; (2) the metallic oxide powder and Al powder are mixed, and then slagging constituents are added; (3) a mixture of the slagging constituents and the powder is put into a reactor, Mg powder is put on a surface layer, under the electromagnetic field effect, open fire ignition is carried out, and a high-temperature melt body is obtained; (4) gold slag smelting is performed on the high-temperature melt body under the electromagnetic field effect, reduction smelting slag on the upper layer is discharged by 30 percent to 50 percent of the total weight, and the smelted high-temperature melt body is obtained; (5) premelting slag is added to carry out refining and impurity removing, meanwhile, deoxidizing agents are injected into the smelted high-temperature melt body, refining slag is removed, and a refining alloy melt body is obtained; (6) forced water cooling is carried out on the refining alloy melt body to be at the room temperature, and then slag removing and ingot extraction are performed. The method is easy to operate, low in requirement for technological conditions, low in cost and capable of rapidly manufacturing large-size immiscible alloy.

Description

technical field [0001] The invention belongs to the technical field of metallurgy, and particularly relates to a method for preparing an immiscible alloy ingot by aluminothermic reduction and slag refining. Background technique [0002] In recent years, with the development of high-power vacuum high-voltage switch technology, CuCr alloy has gradually replaced the traditional W-Cu and Cu-Bi series alloy contact materials due to its advantages of large breaking current capability and high withstand voltage strength. Widely used in high voltage and high power vacuum switch circuit. With the development of ultra-high voltage power transmission, how to prepare homogeneous and large-sized CuCr alloy ingots has become the key to restrict the application of copper-chromium alloy lead materials. [0003] CuCr alloy is a monotectic alloy and cannot be prepared by ordinary smelting method. Therefore, all countries in the world put the development of CuCr alloy preparation technology a...

Claims

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Application Information

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IPC IPC(8): C22B5/04C22B9/10
CPCY02P10/25
Inventor 豆志河张廷安刘燕张子木王聪赵秋月吕国志牛丽萍赫冀成
Owner NORTHEASTERN UNIV
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