Metal three-dimensional, mesh-like porous body for collectors, electrode, and non-aqueous electrolyte secondary battery
A metal porous body, non-aqueous electrolyte technology, applied in the field of current collectors, can solve the problems of high internal resistance, high cost, and the output of lithium ion secondary batteries is not improved, and achieves low internal resistance, reduced manufacturing costs, high output effect
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Embodiment 1
[0142]
[0143] (non-woven fabric)
[0144] Nonwoven fabric (thickness: 1mm, porosity: 94%, unit Area of non-woven fabric weight: 60g / m 2 , 30% cumulative pore diameter (D30): 32 μm).
[0145] (formation of conductive layer)
[0146] Using the sputtering method, on the surface of the obtained non-woven fabric, the weight per unit area is 10g / m 2 To deposit aluminum to form a thin film, thereby forming a conductive layer.
[0147] (Molten Salt Plating)
[0148] A nonwoven fabric having a conductive layer formed on its surface was used as a workpiece. Fix the workpiece on the fixture with power supply function, then place the fixture in the glove box, which has been kept in an argon atmosphere and low humidity environment (dew point: below -30°C), and then immerse the fixture at a temperature of 40 ℃ molten salt aluminum plating bath (composition: 33 mol% of 1-ethyl-3-methylimidazolium chloride (EMIC)-67 mol% of AlCl 3 ). The jig to which the workpiece was fixed was ...
Embodiment 2
[0153]
[0154] "Aluminum porous body 2" was obtained by performing the same operation as in Example 1, except that: as the nonwoven fabric, PP / PE composite fibers (fiber length: 50 mm, fiber diameter: 4.4dTex (25 μm) , core-sheath ratio: 1 / 1) obtained non-woven fabric (thickness: 1mm, porosity: 97%, weight per unit area: 30g / m 2 , 30% cumulative pore diameter ((D30)): 142 μm).
[0155] The porosity of "aluminum porous body 2" was 94%. The 30% cumulative pore diameter (D30) of the "aluminum porous body 2" was 130 μm.
Embodiment 3
[0166]
[0167] Utilize the sputtering method, on the surface of the non-woven fabric used in embodiment 1 with 10g / m 2 A weight per unit area of copper is deposited to form a conductive layer. Next, a copper plating layer is formed on the surface of the nonwoven fabric by electroplating (copper weight per unit area: 400g / m 2 ), thus obtaining "copper-resin composite porous body 1". The obtained "copper-resin composite porous body 1" was heated to remove the nonwoven fabric by firing. Subsequently, the resulting product was heated in a reducing atmosphere to reduce copper, thereby obtaining "copper porous body 1" composed of copper.
[0168] The porosity of "copper porous body 1" was 96%. The 30% cumulative pore diameter (D30) of the "copper porous body 1" was 30 μm.
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Abstract
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