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Light-emitting diode epitaxial wafer growth method

A technology of light-emitting diodes and growth methods, which is applied in the field of growth of light-emitting diode epitaxial wafers, can solve problems such as low softening temperature of glass, and achieve the effects of reducing substrate production costs and increasing production size

Active Publication Date: 2014-12-24
HC SEMITEK CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] In order to solve the problem that glass cannot be used as a material for making GaN-based light-emitting diode chip substrates in the traditional MOCVD method due to its low softening temperature, an embodiment of the present invention provides a method for growing light-emitting diode epitaxial wafers

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  • Light-emitting diode epitaxial wafer growth method
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  • Light-emitting diode epitaxial wafer growth method

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Embodiment 1

[0033] An embodiment of the present invention provides a method for growing a light-emitting diode epitaxial wafer, see figure 1 , the method includes:

[0034] In step S11, the temperature in the reaction chamber is controlled at the first growth temperature, ammonia gas is continuously fed into the reaction chamber and a trimethylgallium source is intermittently fed into the reaction chamber, and an undoped layer is grown on the glass substrate.

[0035] Wherein, the first growth temperature does not exceed 480°.

[0036] In this embodiment, intermittent feeding of the trimethylgallium source may be implemented in the following manner: feeding for 10-50 seconds and intermittently feeding for 2-10 seconds.

[0037] Step S12, adjusting the temperature in the reaction chamber to the second growth temperature, continuously feeding ammonia and silicon sources into the reaction chamber and intermittently feeding trimethylgallium sources, and growing an N-type layer on the undoped...

Embodiment 2

[0048] An embodiment of the present invention provides a method for growing a light-emitting diode epitaxial wafer, see figure 2 , the method includes:

[0049] In step S21, the glass substrate is chemically cleaned and blown dry with a nitrogen gun.

[0050] Specifically, chemical cleaning can be performed in the following ways:

[0051] First, scrub the glass substrate several times with a cotton ball soaked in absolute ethanol, then ultrasonically clean it three times in acetone, each time for 10 min, and then ultrasonically clean it three times in absolute ethanol, each time for 10 min.

[0052] Step S22, placing the glass substrate in a reaction chamber, heating the reaction chamber to an initial temperature under a hydrogen atmosphere, and performing pretreatment on the glass substrate.

[0053] Specifically, the glass substrate can be placed on a graphite disc and sent into the reaction chamber, and the initial temperature is between 410°-440°.

[0054]In step S23, ...

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Abstract

The invention discloses a light-emitting diode epitaxial wafer growth method, and belongs to the technical field of semiconductors. The method includes the steps of controlling the temperature in a reaction cavity to be the first growth temperature, unceasingly injecting ammonia gas into the reaction cavity, intermittently injecting a trimethyl gallium source into the reaction cavity, and growing an undoped layer on a glass substrate; regulating the temperature in the reaction cavity to be the second growth temperature, unceasingly injecting ammonia gas and a silicon source into the reaction cavity, intermittently injecting the trimethyl gallium source into the reaction cavity, and growing an N type layer on the undoped layer; regulating the temperature in the reaction cavity to be the third growth temperature, unceasingly injecting ammonia gas into the reaction cavity, intermittently injecting the trimethyl gallium source and a trimethyl indium source into the reaction cavity, and growing an active layer on the N type layer; regulating the temperature in the reaction cavity to be the fourth growth temperature, unceasingly injecting ammonia gas and a magnesocene source into the reaction cavity, intermittently injecting the trimethyl gallium source into the reaction cavity, and growing a P type layer on the active layer, wherein none of the first growth temperature, the second growth temperature, the third growth temperature and the fourth growth temperature exceeds 480 DEG C.

Description

technical field [0001] The invention relates to the technical field of semiconductors, in particular to a method for growing a light-emitting diode epitaxial wafer. Background technique [0002] Light-emitting diode chip The core component of a light-emitting diode, a light-emitting diode chip mainly includes a substrate, an epitaxial layer grown on the substrate, and electrodes arranged on the epitaxial layer. [0003] At present, GaN-based light-emitting diodes generally use metal-organic chemical vapor deposition (Metal-organic Chemical Vapor Deposition, referred to as "MOCVD") to grow epitaxial layers on the substrate. The commonly used substrate materials are sapphire, silicon carbide and silicon. However, substrates made of these commonly used materials are small in size and high in cost due to substrate warpage, and glass, as a common material, has a lower cost than the above-mentioned commonly used materials. [0004] In the process of realizing the present inventi...

Claims

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Application Information

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IPC IPC(8): H01L33/00
CPCH01L33/0075H01L33/0095H01L2933/0066
Inventor 孙玉芹董彬忠王江波刘榕
Owner HC SEMITEK CORP
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