Nanometer nickel cobalt oxide and preparation method thereof
A nano-cobalt, nickel acid technology, applied in the direction of active material electrodes, structural parts, electrical components, etc., to achieve the effect of reducing cost and improving electrochemical performance
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[0026] Implementation Example 1:
[0027] The first step: ultrasonically dispersing 60 mg of graphite oxide in deionized water for 120 min to obtain a graphene oxide solution;
[0028] In the second step, 0.291g of nickel nitrate and 0.582g of cobalt nitrate were dissolved in 30mL of water and stirred for 60 minutes;
[0029] In the third step, the systems obtained in the first two steps were mixed and stirred for 60 minutes;
[0030] The fourth step, the reaction system of the third step is freeze-dried;
[0031] In the fifth step, the powder obtained after the freeze-drying in the fourth step is heat-treated at 400° C. for 1 hour in a nitrogen atmosphere to obtain two-dimensional coral-shaped nano-nickel cobaltate.
Example Embodiment
[0032] Implementation Example 2:
[0033] The first step: ultrasonically dispersing 20 mg of graphite oxide in deionized water for 30 min to obtain a graphene oxide solution;
[0034] In the second step, 0.291g of nickel nitrate and 0.582g of cobalt nitrate were dissolved in 30mL of water and stirred for 20 minutes;
[0035] In the third step, the systems obtained in the first two steps were mixed and stirred for 30 minutes;
[0036] The fourth step, the reaction system of the third step is freeze-dried;
[0037] In the fifth step, the powder obtained after freeze-drying in the fourth step is heat-treated at 200° C. for 5 hours under a nitrogen atmosphere to obtain two-dimensional coral-shaped nano-nickel cobaltate.
Example Embodiment
[0038] Implementation example 3:
[0039] The first step: ultrasonically dispersing 30 mg of graphite oxide in deionized water for 60 min to obtain a graphene oxide solution;
[0040] In the second step, 0.291g of nickel nitrate and 0.582g of cobalt nitrate were dissolved in 30mL of water and stirred for 30 minutes;
[0041] In the third step, the systems obtained in the first two steps were mixed and stirred for 60 minutes;
[0042] The fourth step, the reaction system of the third step is freeze-dried;
[0043] In the fifth step, the powder obtained after freeze-drying in the fourth step is heat-treated at 300 °C for 2 hours in a nitrogen atmosphere to obtain two-dimensional coral-shaped nano-nickel cobalt oxide. The field emission scanning electron microscope is as follows: figure 2 shown. The prepared two-dimensional coral-like nano-nickel cobalt oxide was used as a negative electrode material for lithium ion batteries to conduct electrochemical performance tests. The ...
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