A kind of production method for preparing ammonium phosphate by-product longan special fertilizer
A production method and technology of ammonium phosphate, which are applied in the directions of phosphate, phosphorus oxyacid, application, etc., can solve the problems of increasing the preparation cost of ammonium phosphate products, affecting the purity of ammonium phosphate products, and low purity of ammonium phosphate products, and achieving remarkable results. Environmental value and economic benefits, improved land utilization, improved yield and quality
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Embodiment 1
[0043] A production method for preparing ammonium phosphate by-product longan special fertilizer, using phosphoric acid and urea to mix at a molar ratio of 1.1:1, stirring and reacting at a temperature of 93°C for 1 hour to obtain an intermediate slurry; Ammonia gas was introduced, and the reaction temperature was controlled to be 70°C. After stirring and reacting for 23 minutes, the pH value of the end point was controlled to be 9.8 to obtain ammonium phosphate slurry; And the nitrogen and phosphorus elements in the solution are detected, analyzed and adjusted so that the molar ratio of the nitrogen and phosphorus elements in the solution is 1.1:1.6, stop crystallization and filter, the filter cake is an ammonium phosphate product, and potassium and phosphorus are added to the filtrate. Medium and trace element compounds, and adjust the molar ratio of nitrogen, phosphorus and potassium elements in the solution to 1.3:1.7:1.1 to obtain the first product of the compound fertiliz...
Embodiment 2
[0051] A production method for preparing ammonium phosphate by-product longan special fertilizer, using phosphoric acid and urea to mix at a molar ratio of 2.4:1, stirring and reacting for 2 hours at a temperature of 113°C to obtain an intermediate slurry; Ammonia gas was introduced, and the reaction temperature was controlled to be 80°C. After stirring and reacting for 33 minutes, the pH value of the end point was controlled to be 11.4 to obtain ammonium phosphate slurry; And the nitrogen and phosphorus elements in the solution are detected, analyzed and adjusted so that after the molar ratio of the nitrogen and phosphorus elements in the solution is 1.1:2.1, the crystallization is stopped and the filtration process is carried out. The filter cake is an ammonium phosphate product, and potassium components and Medium and trace element compounds, and adjust the molar ratio of nitrogen, phosphorus and potassium elements in the solution to 1.3:2.3:1.3 to obtain the first product o...
Embodiment 3
[0059] A production method for preparing ammonium phosphate by-product longan special fertilizer, using phosphoric acid and urea to mix at a molar ratio of 1.7:1, stirring and reacting at a temperature of 98°C for 1.5 hours to obtain an intermediate slurry; Ammonia gas was passed into the medium, and the reaction temperature was controlled at 75°C. After stirring for 28 minutes, the pH value of the end point was controlled to be 10.5 to obtain ammonium phosphate slurry; then the ammonium phosphate slurry was placed in a circulating cooling crystallizer for circulating cooling crystallization treatment , and detect, analyze and adjust the nitrogen and phosphorus elements in the solution so that the molar ratio of the nitrogen and phosphorus elements in the solution is 1.1:1.9, stop crystallization and filter, the filter cake is an ammonium phosphate product, and add potassium to the filtrate and medium and trace element compounds, and adjust the molar ratio of nitrogen, phosphor...
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