A kind of production method for preparing special fertilizer for ammonium phosphate by-product red peony
A production method and technology of ammonium phosphate, which are applied in the directions of ammonium orthophosphate fertilizer, alkaline orthophosphate fertilizer, phosphate fertilizer, etc., can solve the problems of increasing the preparation cost of ammonium phosphate products, less results, soil pollution, etc., and achieve significant environmental protection value. and economic benefits, improving yield and quality, and reducing soil compaction
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Embodiment 1
[0043] A production method for preparing ammonium phosphate by-product Radix Paeoniae Rubra, which uses phosphoric acid and urea to mix at a molar ratio of 1.5:1, and stirs and reacts for 1 hour at a temperature of 90°C to obtain an intermediate slurry; Ammonia gas was passed into the medium, and the reaction temperature was controlled at 60°C. After stirring for 20 minutes, the pH value of the end point was controlled to be 9.8 to obtain ammonium phosphate slurry; then the ammonium phosphate slurry was placed in a circulating cooling crystallizer for circulating cooling crystallization treatment , and the nitrogen and phosphorus elements in the solution are detected, analyzed and adjusted so that the molar ratio of the nitrogen and phosphorus elements in the solution is 1.1:1.1, stop crystallization and filter, the filter cake is an ammonium phosphate product, and potassium components are added to the filtrate and medium and trace element compounds, and adjust the molar ratio ...
Embodiment 2
[0051] A production method for preparing ammonium phosphate by-product Radix Paeoniae Rubra special fertilizer, using phosphoric acid and urea to mix according to the molar ratio of 1.8:1, stirring and reacting at a temperature of 110°C for 2.5 hours to obtain an intermediate slurry; Ammonia gas is introduced into the slurry, and the reaction temperature is controlled at 90°C. After stirring for 30 minutes, the pH value at the end point is controlled to be 11.4 to obtain ammonium phosphate slurry; then the ammonium phosphate slurry is placed in a circulating cooling crystallizer for circulating cooling crystallization treatment, and detect, analyze and adjust the nitrogen and phosphorus elements in the solution so that the molar ratio of the nitrogen and phosphorus elements in the solution is 1.1:1.7, then stop the crystallization and filter the treatment, the filter cake is an ammonium phosphate product, and add potassium to the filtrate Components and trace element compounds,...
Embodiment 3
[0059] A production method for preparing ammonium phosphate by-product red peony root special fertilizer, using phosphoric acid and urea to mix according to the molar ratio of 1.65:1, stirring and reacting for 2 hours at a temperature of 100°C to obtain an intermediate slurry; Ammonia gas was passed into the medium, and the reaction temperature was controlled at 75°C. After stirring for 25 minutes, the pH value of the end point was controlled to be 10.3 to obtain ammonium phosphate slurry; then the ammonium phosphate slurry was placed in a circulating cooling crystallizer for circulating cooling crystallization treatment , and detect, analyze and adjust the nitrogen and phosphorus elements in the solution, so that the molar ratio of the nitrogen and phosphorus elements in the solution is 1.1:1.4, stop the crystallization and filter, the filter cake is ammonium phosphate product, and add potassium to the filtrate and medium and trace element compounds, and adjust the molar ratio...
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