A kind of uv ultraviolet light curing glue and preparation method thereof
A technology of curing glue and ultraviolet light, applied in the direction of adhesive type, ester copolymer adhesive, etc., can solve the problem of high cost performance of products, and achieve the effect of low cost and excellent comprehensive performance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0031] In a 5000ml reaction bottle, put 3000g of NPGDA first, then 1250g of DPGDA, start stirring, raise the temperature to 60°C, then add 600g of TMPTA, and then add 50g of photoinitiator 184. Keep the temperature at 60°C, stir for 2 hours, and then filter through a 0.1um filter to obtain the product. Yield 100%.
Embodiment 2
[0033] In a 5000ml reaction bottle, put 3000g of NPGDA first, then 1100g of DPGDA, start stirring, raise the temperature to 55°C, then add 550g of TMPTA, and then add 50g of photoinitiator 184. Keep the temperature at 55°C, stir for 2.5 hours, and then filter through a 0.1um filter to obtain the product. Yield 100%.
Embodiment 3
[0035] In a 5000ml reaction bottle, put 3000g of NPGDA first, then 1300g of DPGDA, start stirring, raise the temperature to 65°C, then add 700g of TMPTA, and then add 55g of photoinitiator 184. Keep the temperature at 65°C, stir for 1.5 hours, and then filter through a 0.1um filter to obtain the product. Yield 100%.
[0036] The UV curable adhesives of Examples 1 to 3 are coated on the surface of polycarbonate plastic sheets by spin coating, cured by ultraviolet light to form a coating film, and the performance of the coating film is tested. The results show that the results of Examples 1 to 3 All UV curable adhesives have a good appearance, the adhesion is grade 1 (tested according to GB / T9286-1998, the evaluation results are divided into 5 grades, 0 is the best, and 5 is the worst), and the hardness is above grade B (according to GB / T9286-1998 / T6739-1996 method detection), acid resistance (the test board is immersed in 5% sulfuric acid at 25 ° C, and the appearance is good...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 