Antibacterial printing ink composition and preparation method thereof
A technology of ink composition and antibacterial agent, applied in ink, household utensils, applications, etc., can solve problems affecting health, cross-infection, etc., and achieve good coating or printing effects, low cost, and excellent adhesion.
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[0030] Example 1
[0031] (1) Take carbon black 5kg, add trimethoprim 0.29kg, nano-titanium dioxide 0.58kg, nano-zinc oxide 1.16kg, diglycidyl phthalate 11kg, 1-hydroxycyclohexyl phenylacetone 8kg and Propylene oxide butyl ether 11kg, mix well;
[0032] (2) Take by weighing 6 kg of sodium dibutylnaphthalene sulfonate, 3 kg of polydimethylsiloxane, 3.5 kg of Tween 20 and 1.5 kg of polyepoxysuccinic acid, and add it to a three-roll mill and grind for 15 minutes;
[0033] (3) The product of step 1 and the product of step 2 were ultrasonicated at 55° C. for 15 minutes, and degassed under vacuum for 1 hour to obtain an antibacterial ink composition.
[0034] The performance test results of the prepared antibacterial ink composition are shown in Table 1.
Example Embodiment
[0035] Example 2
[0036] (1) Take by weighing 8kg Pigment Yellow 74, add nano titanium dioxide 3kg, diglycidyl phthalate 8kg, 1-hydroxycyclohexyl phenylacetone 11kg and propylene oxide butyl ether 8kg successively, mix uniformly;
[0037] (2) Take by weighing 4kg of sodium dibutylnaphthalene sulfonate, 3kg of polydimethylsiloxane, 5kg of Tween 60 and 2kg of polyepoxysuccinic acid, and add it to a three-roll mill and grind for 10 minutes;
[0038] (3) The product of step 1 and the product of step 2 were ultrasonicated at 60° C. for 20 minutes, and defoamed for 2 hours under vacuum conditions to obtain an antibacterial ink composition.
[0039] The performance test results of the prepared antibacterial ink composition are shown in Table 1.
Example Embodiment
[0040] Example 3
[0041] (1) Take by weighing 6kg Pigment Yellow 155, add trimethoprim 2kg, diglycidyl phthalate 11kg, 1-hydroxycyclohexyl phenylacetone 10kg and propylene oxide butyl ether 9kg successively, mix well;
[0042] (2) Take by weighing 7kg of sodium dibutylnaphthalene sulfonate, 2kg of polydimethylsiloxane, 3.5kg of Tween 40 and 1.5kg of polyepoxysuccinic acid, and add it to a three-roll mill and grind for 20 minutes;
[0043] (3) The product of step 1 and the product of step 2 were ultrasonicated at 70° C. for 25 minutes, and defoamed under vacuum for 2 hours to obtain an antibacterial ink composition.
[0044] The performance test results of the prepared antibacterial ink composition are shown in Table 1.
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