Unlock instant, AI-driven research and patent intelligence for your innovation.

A method for reducing the viscosity of quenching oil in an ethylene plant

An ethylene plant and quench oil technology, which is applied in the direction of multi-stage series refining process treatment, can solve the problems of unstable operation of the quench oil visbreaking system, low heat recovery efficiency, viscosity reduction effect, etc., and achieve the reduction of solvent circulation. , Improve the effect of reducing viscosity, reduce the effect of viscosity

Active Publication Date: 2016-05-25
CHINA PETROLEUM & CHEM CORP +1
View PDF5 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The disadvantages of this method are: first, when the ethane furnace burns, it must be stripped with high-pressure steam, and the gas phase directly returns to the quenching oil tower, and the load of the quenching oil tower is high; second, the light components in the heavy fuel oil are sent outside after stripping The content is small, and the outgoing pipeline is prone to blockage
This method only optimizes the temperature distribution of the oil scrubber, does not change the composition of the quenching oil, has little effect on reducing the viscosity, and increases the load in the middle section of the oil scrubber, affecting production capacity
[0010] Although the above method can partially reduce the viscosity of the quenching oil, it cannot fundamentally solve the problem of high viscosity of the quenching oil
At present, many ethylene plants in China have unreasonable design of the quenching oil visbreaking system, high viscosity of the quenching oil, high temperature at the top of the quenching oil tower, low temperature at the bottom of the tower, unstable operation of the quenching oil visbreaking system, and low heat recovery efficiency. Frequent emulsification of quenching water

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A method for reducing the viscosity of quenching oil in an ethylene plant

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] Using propane as solvent, the quench oil is subjected to solvent extraction and viscosity reduction treatment. The feed temperature of quenching oil is 90°C, the pressure is 10MPa, and the flow rate is 10t / h. The solvent feed temperature is 90°C, the pressure is 10MPa, the flow rate is 19t / h, and the weight ratio of solvent to quench oil is 1.9. Quenching oil and 0.05 times its weight of solvent enter from the upper part of the extraction tower, and the remaining solvents enter from the lower part of the extraction tower. The temperature of the extraction tower is 90°C and the pressure is 10MPa. The extraction oil is separated from the top of the extraction tower, and the raffinate is separated from the bottom of the tower. The asphalt phase is decompressed to 0.8MPa atmospheric pressure to remove the solvent, and then it is recovered as fuel oil.

[0036] Reduce the pressure of the extracted oil flowing out from the top of the extraction tower to 0.8MPa, adjust the ...

Embodiment 2

[0038] Using propane as solvent, the quench oil is subjected to solvent extraction and viscosity reduction treatment. The feed temperature of quenching oil is 70°C, the pressure is 5MPa, and the flow rate is 10t / h. The solvent feed temperature is 70°C, the pressure is 5MPa, the flow rate is 10t / h, and the weight ratio of solvent to quench oil is 1. Quenching oil and 0.05 times its weight of solvent enter from the upper part of the extraction tower, and the remaining solvents enter from the lower part of the extraction tower. The temperature of the extraction tower is 70°C and the pressure is 5MPa. The extraction oil is separated from the top of the extraction tower, and the raffinate is separated from the bottom of the tower. The asphalt phase is decompressed to 0.8MPa atmospheric pressure to remove the solvent, and then it is recovered as fuel oil.

[0039] Reduce the pressure of the extracted oil flowing out from the top of the extraction tower to 0.8MPa, adjust the tempe...

Embodiment 3

[0041] Using propane as solvent, the quench oil is subjected to solvent extraction and viscosity reduction treatment. The feed temperature of quenching oil is 30°C, the pressure is 5MPa, and the flow rate is 10t / h. The solvent feed temperature is 30° C., the pressure is 5 MPa, the flow rate is 5 t / h, and the weight ratio of total solvent to quench oil is 0.5. Quenching oil and 0.05 times its weight of solvent enter from the upper part of the extraction tower, and the remaining solvents enter from the lower part of the extraction tower. The temperature of the extraction tower is 30°C and the pressure is 5MPa. The extraction oil is separated from the top of the extraction tower, and the raffinate is separated from the bottom of the tower. The asphalt phase is depressurized to 0.5MPa to remove the solvent and then produced as fuel oil.

[0042] Reduce the pressure of the extracted oil flowing out of the top of the extraction tower to 0.5MPa, adjust the temperature to 30°C, and...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
viscosityaaaaaaaaaa
Login to View More

Abstract

The invention discloses a method for reducing ethylene unit quenching oil viscosity. The method comprises solvent-based extraction of quenching oil from an ethylene unit, and solvent recovery for viscosity-reduced quenching oil acquisition. A weight ratio of the solvent to the quenching oil in solvent-based extraction is 0.01-1.99 and preferably is 0.5-1.99. The method comprises the following steps of 1, solvent-based extraction: introducing quenching oil from an ethylene unit, carrying out solvent-based extraction in an extraction tower, separating extract oil from the tower top and separating raffinate asphalt from the top bottom, and 2, solvent recovery: carrying out heating and / or pressure reduction on the extract oil obtained by the step 1, feeding the extract oil into a solvent recovery tower and separating a solvent and viscosity-reduced quenching oil. The method greatly reduces ethylene unit quenching oil viscosity. The method utilizes a low solvent ratio in solvent extraction so that visbreaking effects are improved, a solvent circulation volume is greatly reduced and energy consumption is reduced.

Description

technical field [0001] The invention relates to the field of ethylene production, and more particularly relates to a method for reducing the viscosity of quenching oil in an ethylene unit. Background technique [0002] At present, major ethylene plants in the world use steam pyrolysis to produce basic organic chemical raw materials such as ethylene, propylene, butadiene, and aromatics. Raw materials such as light hydrocarbons, naphtha, and hydrogenated tail oil are mixed with a certain proportion of diluted steam in an industrial cracking furnace to undergo cracking reactions under high temperature conditions. Diene and other chemical raw materials. [0003] The quenching system is an important part of the ethylene plant. It is composed of quenching cooler, oil washing tower, water washing tower and other equipment. As the first process of ethylene cracking gas treatment, it often becomes the bottleneck restricting the output and long-term stable operation of the ethylene ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C10G53/04
CPCC10G53/04
Inventor 刘同举杜志国王国清郭莹张永刚杨晓红
Owner CHINA PETROLEUM & CHEM CORP