Fingerprint detection method for antitumor traditional Chinese medicine composition
A technology of fingerprint spectrum and detection method, which is applied in the field of fingerprint spectrum detection of traditional Chinese medicine compositions, can solve the problems such as the inability to comprehensively and objectively detect and evaluate the quality of Tianfoshen oral liquid.
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Embodiment 1
[0116] 1. A fingerprint detection method of an anti-tumor Chinese medicinal composition, in parts by weight, the Chinese medicinal composition is composed of 50 parts of American ginseng, 0.25 part of toad venom, 167 parts of Asparagus, 200 parts of Fritillaria, and oval leaf. 599 parts of Wujia, 1,000 parts of kiwi fruit root, 333 parts of sea buckthorn fruit, and 167 parts of bergamot were prepared into oral liquid preparations. The fingerprint detection method includes the following steps:
[0117] (1) Preparation of the test solution: take the traditional Chinese medicine composition and process it by an appropriate method to make the test solution;
[0118] (2) Determination of the reference fingerprint of this product by high performance liquid chromatography: take more than 10 batches of Chinese medicine composition test samples and inject them under appropriate chromatographic conditions, measure the fingerprints of each batch of test samples, and use these fingerprints...
Embodiment 2
[0130] A fingerprint detection method for an anti-tumor traditional Chinese medicine composition, calculated in parts by weight, the traditional Chinese medicine composition is composed of 50 parts of American ginseng, 0.25 parts of toad venom, 167 parts of Asparagus, 200 parts of Fritillaria, and Ovii 599 parts, 1000 parts of kiwi fruit roots, 333 parts of sea buckthorn fruit, and 167 parts of bergamot were prepared into oral liquid preparations. The fingerprint detection method includes the following steps:
[0131] (1) Preparation of the test solution: take the traditional Chinese medicine composition and process it by an appropriate method to make the test solution;
[0132] (2) Determination of the reference fingerprint of this product by high performance liquid chromatography: take more than 10 batches of Chinese medicine composition test samples and inject them under appropriate chromatographic conditions, measure the fingerprints of each batch of test samples, and use t...
Embodiment 3
[0145] A fingerprint detection method for an anti-tumor traditional Chinese medicine composition, calculated in parts by weight, the traditional Chinese medicine composition is composed of 60 parts of American ginseng, 0.30 parts of toad venom, 180 parts of Asparagus, 210 parts of Fritillaria, and Ovale vulgaris 620 parts, 1100 parts of kiwi fruit roots, 340 parts of sea buckthorn fruit, and 210 parts of bergamot were prepared into oral liquid preparations. The fingerprint detection method includes the following steps:
[0146] (1) Preparation of the test solution: take the traditional Chinese medicine composition and process it by an appropriate method to make the test solution;
[0147] (2) Determination of the reference fingerprint of this product by high performance liquid chromatography: take more than 10 batches of Chinese medicine composition test samples and inject them under appropriate chromatographic conditions, measure the fingerprints of each batch of test samples,...
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