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A kind of quality detection method of antitumor traditional Chinese medicine composition

A detection method and composition technology, applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of inability to comprehensively and objectively detect and evaluate the quality of Tianfoshen Oral Liquid

Active Publication Date: 2016-06-15
常熟雷允上制药有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, Acanthopanax ovalifolia, kiwi fruit root, and sea buckthorn fruit are extracted by water extraction process, and American ginseng, asparagus, and soil Fritillaria are extracted by alcohol extraction process. The polarity of the compounds contained in the total extract covers the range of strong polarity and medium polarity. The detection methods of the prior art cannot comprehensively and objectively detect and evaluate the quality of Tianfoshen Oral Liquid

Method used

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  • A kind of quality detection method of antitumor traditional Chinese medicine composition
  • A kind of quality detection method of antitumor traditional Chinese medicine composition
  • A kind of quality detection method of antitumor traditional Chinese medicine composition

Examples

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Embodiment 1

[0143] A quality detection method of an anti-tumor traditional Chinese medicine composition, the traditional Chinese medicine composition is composed of 50 parts of American ginseng, 0.25 parts of toad venom, 167 parts of asparagus, 200 parts of Scutellaria fritillaria, 599 parts of Aminocystis acanthus, and 1000 parts of kiwi fruit root , 333 parts of seabuckthorn fruit, 167 parts of bergamot are made into oral liquid preparation, it is characterized in that, described detection method comprises the TLC identification of bergamot and American ginseng, comprises the following steps:

[0144] The TLC identification of bergamot includes the following steps:

[0145] (1) Preparation of need testing solution: get 20ml of Chinese medicine composition, add ethyl acetate to extract three times, each 15ml, combine ethyl acetate extract, concentrate to about 2ml on the water bath, to obtain final product;

[0146] (2) Preparation of reference substance solution: take 1 g of bergamot re...

Embodiment 2

[0186] 1. A quality detection method for an anti-tumor Chinese medicine composition. In parts by weight, the Chinese medicine composition is composed of 40 parts of American ginseng, 0.22 parts of toad venom, 160 parts of asparagus, 190 parts of S. Add 560 parts, 900 parts of kiwifruit roots, 320 parts of seabuckthorn fruit, and 190 parts of bergamot to make oral liquid preparations, it is characterized in that, the detection method comprises the TLC identification of bergamot and American ginseng, comprising the following steps:

[0187] The TLC identification of bergamot includes the following steps:

[0188] (1) Preparation of the test solution: get 60ml of the Chinese medicine composition, add ethyl acetate to extract three times, each 45ml, combine the ethyl acetate extract, concentrate on a water bath to about 4ml, to obtain final product;

[0189] (2) Preparation of reference substance solution: take bergamot reference drug powder 5g, add volume concentration 80% ethano...

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Abstract

The invention discloses a quality detection method of an anti-tumour traditional Chinese medicine composition. The method comprises thin-layer chromatography of fingered citron and American ginseng, a high performance liquid chromatography content determination method of American ginseng and venenum bufonis, and a finger-print detection method of the traditional Chinese medicine composition. The detection method provided by the invention is capable of comprehensively, objectively and accurately detecting and evaluating the quality of the anti-tumour traditional Chinese medicine composition and is of great significance for guaranteeing clinical efficacy.

Description

technical field [0001] The invention relates to a quality detection method of a traditional Chinese medicine composition, in particular to a quality detection method of a traditional Chinese medicine composition with antitumor effect. Background technique [0002] Tianfoshen oral liquid is a pure natural traditional Chinese medicine preparation refined and refined by modern advanced technology. It is produced by Changshu Leiyunshang Pharmaceutical Co., Ltd. It has the effects of nourishing yin and replenishing qi, detoxifying and dispelling stagnation, and it is used in combination with anti-tumor chemicals It is used for non-small cell lung cancer with deficiency of both qi and yin, and can relieve nausea, vomiting, constipation, hair loss and other phenomena caused by chemotherapy. It has been widely used in clinical practice, and its curative effect is accurate and reliable. Among them, Tianfoshen Oral Liquid is composed of 8 medicinal materials: American ginseng, toad ve...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90G01N30/88
Inventor 顾治平阙瑞艳王恒斌陈力建张礼学
Owner 常熟雷允上制药有限公司
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