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Preparation method and application of florists chrysanthemum extract

A technology of extract and chrysanthemum, applied in the field of cigarette additive processing, can solve problems such as unreported, and achieve the effects of improving smoke characteristics, good solubility and convenient application

Inactive Publication Date: 2015-04-08
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

So far, there has been no report on the use of tribute chrysanthemum extracts as flavoring spices for cigarette filter sticks

Method used

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  • Preparation method and application of florists chrysanthemum extract

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] After washing and drying the fresh chrysanthemum, weigh 100 grams of the dried chrysanthemum, crush it into chrysanthemum powder with a particle size less than or equal to 5mm, and place it in the extraction kettle; the added weight is 0.2 times the weight of the chrysanthemum powder The ethanol is used as the extraction aid, and the extraction kettle is sealed after stirring evenly; the temperature in the extraction kettle is set at 30°C, the pressure is 40MPa, and the flow rate of 15kg / h CO 2 , extract for 2.5h, collect the extract, and filter to obtain the prepared chrysanthemum extract.

[0019] After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter stick according to the added amount of 0.05‰ of the tow mass, compared with the original finished cigarette, and experts were invited to conduct sensory evaluation. The evaluation results are shown in Table 1.

Embodiment 2

[0021] After washing and drying the fresh chrysanthemum, weigh 100 grams of the dried chrysanthemum, crush it into a tribute chrysanthemum powder with a particle size less than or equal to 5mm, and place it in an extraction kettle; the added weight is 1 times the weight of the tribute chrysanthemum powder The ethanol is used as the extraction aid, and the extraction kettle is sealed after stirring evenly; the temperature in the extraction kettle is set at 40°C, the pressure is 20MPa, and the flow rate of 5kg / h CO 2 , extract for 5h, collect the extract, and filter to obtain the prepared chrysanthemum extract.

[0022] After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter stick according to the added amount of 0.1‰ of the tow mass, compared with the original finished cigarette, and experts were invited to conduct sensory evaluation. The evaluation results are shown in Table 1.

Embodiment 3

[0024] After washing and drying the fresh chrysanthemum, weigh 100 grams of the dried chrysanthemum, crush it into a tribute chrysanthemum powder with a particle size less than or equal to 5mm, and place it in the extraction kettle; the added weight is 0.3 times the weight of the tribute chrysanthemum powder The ethanol is used as the extraction aid, and the extraction kettle is sealed after stirring evenly; the temperature in the extraction kettle is set at 60°C, the pressure is 20MPa, and the flow rate of 8kg / h CO 2 , extract for 0.5h, collect the extract, and filter to obtain the prepared chrysanthemum extract.

[0025] After dissolving the extract with glyceryl triacetate, it was sprayed on the cigarette filter stick according to the added amount of 0.3‰ of the tow mass, compared with the original finished cigarette, and experts were invited to conduct sensory evaluation. The evaluation results are shown in Table 1.

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Abstract

The invention discloses a preparation method and application of a florists chrysanthemum extract. The preparation method comprises the steps of drying fresh florists chrysanthemum taken as the raw material; crushing; performing supercritical CO2 extraction; filtering to obtain the florists chrysanthemum extract; dissolving the florists chrysanthemum extract with glycerol triacetate; spraying to tobacco shred based on the dosage of 0.05 to 0.9 per mill. The florists chrysanthemum extract prepared by the method is used for perfuming cigarette filter tips, and can be used for effectively improving the smoke flavor characteristic, in particular improving the flowery flavor and sweetness of cigarettes with faint scent, and the irritation of smoke can be reduced to certain extent.

Description

technical field [0001] The invention belongs to the technical field of cigarette additive processing, and in particular relates to a preparation method of tribute chrysanthemum extract. At the same time, the invention also relates to the application of the tribute chrysanthemum extract in flavoring cigarette filter sticks. Background technique [0002] According to reports, chrysanthemum is rich in phytochemical components, mainly glycosides represented by acacetin-7-O-β-D-galactopyranoside, cosmoside, luteolin, etc., and glycosides represented by β -Monoterpenes, sesquiterpenes, triterpenes and other terpenoids represented by phellandrene, p-cymene, inrenone, 1,8-cineole, borneol, and sabinene. These phytochemical components, many The same aroma components as tobacco plants. Among them, tribute chrysanthemum is one of the four famous chrysanthemums in my country. The formation and transformation of its aroma compounds are more sufficient and higher in content than other c...

Claims

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Application Information

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IPC IPC(8): C11B9/02A24B15/30
CPCC11B9/025A24B15/30
Inventor 余耀丁海燕詹建波李赓张莹余振华余婷婷
Owner CHINA TOBACCO YUNNAN IND