Aerogel material and preparation method and application thereof
An aerogel and sustained-release material technology, which is applied in the field of aerogel materials and its preparation, can solve the problems of uneven release speed, insufficient sustained-release time, and inability of consumers to add mosquito repellents at will, and achieves liquid release. Uniform speed, excellent sustained release performance, no toxic and side effects
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Embodiment 1
[0044] (1) Weigh raw materials: Weigh 33 grams of hexamethylene diisocyanate trimer (Desmodur N3300A), 94 ml of polar solvent acetone, 3.53 ml of deionized water, and 0.6% by mass of alkali Sex catalyst triethylamine (Triethylamine);
[0045] (2) Mixing: First, mix the hexamethylene diisocyanate trimer and acetone weighed in step (1) evenly, then add deionized water to the mixed solution, then add the basic catalyst triethylamine, and mix evenly;
[0046] (3) Post-processing: Stir the mixture obtained in step (2) uniformly with a magnetic bar stirrer for 10 minutes, then let it stand for 1 hour to form an airgel, and inject the airgel into a polypropylene plastic mold to form and dry An airgel material is obtained.
[0047] The density of the airgel material prepared in Example 1 is about: 0.33g / cm 3 , is a high-density airgel material.
Embodiment 2
[0049] (1) Weigh raw materials: Weigh 17 grams of hexamethylene diisocyanate trimer (Desmodur N3300A), 94 ml of polar solvent acetone, 1.5 ml of deionized water, and 0.2% by mass of alkali Sex catalyst triethylamine (Triethylamine);
[0050] (2) Mixing: First, mix the hexamethylene diisocyanate trimer and acetone weighed in step (1) evenly, then add deionized water to the mixed solution, then add the basic catalyst triethylamine, and mix evenly;
[0051] (3) Post-processing: Stir the mixture obtained in step (2) evenly for 10 minutes with a magnetic bar stirrer, and then let it stand for 3 hours to form an airgel, and inject the airgel into a polypropylene plastic mold to form and dry An airgel material is obtained.
[0052] The density of the airgel material prepared in embodiment 2 is about: 0.17g / cm 3 , is a medium-density airgel material.
Embodiment 3
[0054] (1) Weigh raw materials: Weigh 7 grams of hexamethylene diisocyanate trimer (Desmodur N3300A), 94 ml of polar solvent acetonitrile, 0.2 ml of deionized water, and 0.05% by mass of alkali Sex catalyst triethylamine (Triethylamine);
[0055] (2) Mixing: First, mix the hexamethylene diisocyanate trimer and acetone weighed in step (1) evenly, then add deionized water to the mixed solution, then add the basic catalyst triethylamine, and mix evenly;
[0056] (3) Post-processing: Stir the mixture obtained in step (2) evenly for 10 minutes with a magnetic bar stirrer, and then let it stand for 12 hours to form an airgel, and inject the airgel into a polypropylene plastic mold to form and dry An airgel material is obtained.
[0057] The density of the airgel material prepared in embodiment 3 is about: 0.07g / cm 3 , is a low-density airgel material.
[0058] figure 1 It is the electron micrograph of the airgel material prepared in Example 1.
[0059] Such as figure 1 Shown...
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