A treatment method of nano-silica particles for oil drag reducer
A technology of nano-silica and silica, which is applied in dyeing organosilicon compound treatment, dyeing physical treatment, fibrous filler, etc., can solve the problems of loss of drag reduction function and molecular weight reduction, etc., to improve compound efficiency and enhance The effect of strength and toughness
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[0025] Dissolve 20g of n-heptane in 100g of N-methylpyrrolidone to prepare a dispersion, place it in a 25khz ultrasonic environment, take 50g of nano-silica with a specific surface area of 640m2 / g and a primary particle size of 10nm, and make the nano-silica Silicon was added in 5 times, the mass order of adding was 20g, 15g, 7.5g, 5g, 2.5g, each interval was 5min, and ultrasonic was 30min. Prepare the compound type I silane coupling agent according to the mass ratio of KH-550 and KH-570 of 3:1, and prepare the compound type II silane according to the mass ratio of KH-550, KH-560 and A-172 in the ratio of 5:3:1 coupling agent. Prepare the modifier according to the mixing mass ratio of type I silane coupling agent, modifier additive and deionized water as 100:10:5. Divide 2g of modifier into 5 times, add 0.4g each time to the dispersion, refrigerate at -30°C for 5h, and stir at 60rad / min at a constant temperature of 40°C for 6h. Centrifuge three times, wash and filter each ...
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