Cynanchum atratum extract as well as preparation method and application thereof
An extract, the technology of Bai Wei, which is applied in the field of Bai Wei extract and its preparation, can solve the problems that have not been reported on the role of pathogenic fungi in postharvest citrus, achieve the effects of shortening extraction costs, good application prospects, and improving product quality
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Embodiment 1
[0051] Embodiment 1 A kind of Baiwei extract
[0052] The Baiwei extract is prepared by the following steps:
[0053] 1. Baiwei is dried at 40 ℃, and after pulverizing, cross a 40-mesh sieve, and get the powder under the sieve;
[0054] II. in the powder that step 1 obtains, adding the weight percent concentration of 10 times of described Baiwei weight is 95% ethanol to carry out ultrasonic-assisted extraction, extraction temperature is 40 ℃, extraction time is 2 hours, and ultrasonic frequency is 30KHz; Filter, obtain alcohol extract;
[0055] III. In the alcohol extract obtained in step II, ethanol is recovered under reduced pressure until there is no alcohol smell, and the target product is obtained.
Embodiment 2
[0056] Embodiment 2 A kind of Baiwei extract
[0057] The Baiwei extract is prepared by the following steps:
[0058] 1. Dry Baiwei at 50 °C, cross a 40-mesh sieve after pulverizing, and get the powder under the sieve;
[0059] II. in the powder that step 1 obtains, adding the weight percent concentration of 20 times of described Baiwei weight is 40% ethanol to carry out ultrasonic-assisted extraction, extraction temperature is 50 ℃, extraction time is 2 hours, and ultrasonic frequency is 30KHz; Filter, obtain alcohol extract;
[0060] III. The alcohol extract obtained in step II, recover ethanol under reduced pressure until there is no alcohol smell to obtain the target product.
Embodiment 3
[0061] Embodiment 3 A kind of Baiwei extract
[0062] The Baiwei extract is prepared by the following method:
[0063] 1. Dry Baiwei at 50 °C, cross a 40-mesh sieve after pulverizing, and get the powder under the sieve;
[0064] II. in the powder that step 1 obtains, adding the weight percent concentration of 20 times of described Baiwei weight is 40% ethanol to carry out ultrasonic-assisted extraction, extraction temperature is 50 ℃, extraction time is 2 hours, and ultrasonic frequency is 30KHz; Filter, obtain Ethanol extract;
[0065] III. the ethanol extract that step II obtains, ethanol is reclaimed under reduced pressure to have no alcohol smell, and the ethanol extract of Baiwei is obtained;
[0066] IV. the described Baiwei ethanol extract that step III obtains is dissolved in the distilled water of 10 times of amounts (weight), after with the ethyl acetate extraction of the equal volume of distilled water three times, then use the n-butanol of equal volume to extract...
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