A kind of water-based ink of modified nano-sepiolite composite water-based amino resin and preparation method thereof
A technology of water-based amino resin and nano sepiolite, which is applied in the direction of ink, chemical instruments and methods, dyeing organosilicon compound treatment, etc., can solve the problems of thermal stability, smoothness and gloss of ink to be improved, and achieve good gloss Degree, the effect of improving the degree of combination
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Embodiment 1
[0033] (1) Preparation of modified nano sepiolite
[0034] Add 1 part of nano-sepiolite with a particle size of 30 nm in 35 parts of water and stir evenly to obtain a nano-sepiolite suspension. After heating the nano-sepiolite suspension to 70 ° C, add 2.5 parts of octadecyl ammonium salt, Continue to heat and stir for 2 hours to obtain liquid A for later use.
[0035] In addition, 4 parts of silane coupling agent KH-550 were weighed and added to 35 parts of ethanol aqueous solution with a concentration of 85wt% for hydrolysis. After 0.5h, a silane coupling agent hydrolyzate was obtained, and the silane coupling agent hydrolyzate was added to the Stirring was continued in liquid A for 2.5 hours, and finally the obtained liquid was subjected to suction filtration, washing, and drying successively to obtain modified nano sepiolite. The parts of the above substances are all parts by weight.
[0036] (2) Preparation of water-based ink
[0037] The parts by mass of each componen...
Embodiment 2
[0048] (1) Preparation of modified nano sepiolite
[0049] Add 1 part of nano-sepiolite with a particle size of 20 nm in 30 parts of water and stir evenly to obtain a nano-sepiolite suspension, heat the nano-sepiolite suspension to 60 ° C, and then add 2 parts of octadecyl ammonium salt, Continue to insulate and stir for 2 hours to obtain liquid A for later use.
[0050] In addition, 3 parts of silane coupling agent KH-570 were weighed and added to 30 parts of ethanol aqueous solution with a concentration of 90wt% for hydrolysis. After 1 hour, a silane coupling agent hydrolyzate was obtained, and the silane coupling agent hydrolyzate was added to the liquid In A, continue to stir for 2 hours, and finally the obtained liquid is successively subjected to suction filtration, washing, and drying to obtain modified nano sepiolite. The parts of the above substances are all parts by weight.
[0051] (2) Preparation of water-based ink
[0052] The parts by mass of each component of...
Embodiment 3
[0063] (1) Preparation of modified nano sepiolite
[0064] Add 1 part of nano-sepiolite with a particle size of 40 nm in 40 parts of water and stir evenly to obtain a nano-sepiolite suspension. After heating the nano-sepiolite suspension to 80 ° C, add 3 parts of octadecyl ammonium salt, Continue to insulate and stir for 2 hours to obtain liquid A for later use.
[0065] In addition, 5 parts of silane coupling agent KH-590 were weighed and added to 40 parts of ethanol aqueous solution with a concentration of 80wt% for hydrolysis. After 0.75h, a silane coupling agent hydrolyzate was obtained, and the silane coupling agent hydrolyzate was added to the Stirring was continued in liquid A for 3 hours, and finally the obtained liquid was subjected to suction filtration, washing, and drying to obtain modified nano sepiolite. The parts of the above substances are all parts by weight.
[0066] (2) Preparation of water-based ink
[0067] The parts by mass of each component of the water...
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