Preparation method of ambroxol hydrochloride nanoparticles
A technology of ambroxol hydrochloride and nanoparticles, which is applied in the field of preparation of ambroxol hydrochloride nanoparticles, and achieves the effects of low production cost, rapid hydrolysis and strong stability
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[0026] Ambroxol hydrochloride nanoparticles were prepared by emulsion polymerization with n-butyl cyanoacrylate as capsule material.
[0027] First, use 10ml of n-butyl polycyanoacrylate in an appropriate amount of ethanol and set aside. Then, accurately measure 50ml of 7.5mg / ml ambroxol hydrochloride solution, add 0.2-2.0g of surfactant Pluronic F-68, 0.2-2.0g of dextran-70, 1-10g of sodium sulfite, and adjust the pH value with hydrochloric acid To 1.0-3.0, spare. Finally, slowly add (1) to (2) under the condition of 50-300r / min, continue to stir for 1-6h, then adjust the pH value to neutral with sodium hydroxide solution, continue to stir for 1-3h, 0.45μm Filter through a microporous membrane to obtain a milky white suspension of ambroxol hydrochloride nanoparticles.
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