hair care composition
A technology of composition and water-based composition, which is applied in hair care, cosmetics, cosmetic preparations, etc., and can solve problems such as reduced efficacy and difficult-to-decompose products
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[0143] Synthesis of associative monomers
[0144]
[0145] Under a nitrogen atmosphere the 35P (150 g) was dissolved in 500 ml dry dichloromethane and cooled to 5°C in an ice bath. Triethylamine (18.6 g) was added via syringe, followed by methacryloyl chloride (20.9 g) dropwise over 30 minutes. After the addition was complete, the solution was warmed to room temperature and stirred for 4 weeks. The solution was then filtered to remove the formed precipitate, washed once with saturated sodium bicarbonate solution (200 ml) and once with saturated brine (200 ml). The solution was then passed through a column containing basic alumina, then the product was dried over anhydrous magnesium sulfate, filtered and the solvent was removed in vacuo. The product is referred to as Surfmer D1 in the examples that follow.
[0146] Synthesis of HASE Copolymer
[0147] To a round bottom flask was charged ethyl acrylate (66.8 g), methacrylic acid (37.7 g), maleic anhydride (0.515 g) an...
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