Application of sargassum.graminifolium.turn extracts in caries prevention oral care articles
A technology of Sargassum vulgare and extract, which is applied in the directions of oral care, cosmetic preparations, cosmetic preparations, etc., to achieve the effects of high extraction rate, removal of tooth stains, and small loss of biological activity
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Embodiment 1
[0037] The preparation of embodiment 1 Sargassum herbaceous polysaccharide extract and Sargassum herbaceous polyphenol extract (1)
[0038] 1. Method steps
[0039] 1.1 Simultaneous extraction of Sargassum sargassum polysaccharide extract and Sargassum sargassum polyphenol extract
[0040] (1) Remove impurities from the raw material Sargassum sargassum and wash it with water, put the cleaned Sargassum sargassum into a drying box, dry at 30°C for 20 hours to constant weight, and then put the dried Sargassum sargassum in Pulverize in a pulverizer to obtain powder, pass through a 20-mesh sieve to obtain dry powder of Sargassum grassa, and freeze for future use.
[0041] (2) Add ethanol with a volume fraction of 80% to the dry powder of Sargassum sargassum, and then reflux for extraction for about 3 hours. After the reflux, filter out the ethanol, then place the Sargassum sargassum powder in a fume hood to completely volatilize the ethanol, and finally dry the Sargassum sargassu...
Embodiment 2
[0076] The preparation of embodiment 2 Sargassum herbaceous polysaccharide extract and Sargassum herbaceous polyphenol extract (two)
[0077] 1. Method steps
[0078] (1) Remove impurities from the raw material Sargassum sargassum and wash it with water, put the cleaned Sargassum sargassum into a drying box, dry at 20°C for 24 hours to constant weight, and then put the dried Sargassum sargassum in Pulverize in a pulverizer to obtain powder, pass through a 40-mesh sieve to obtain dry powder of Sargassum grassa, and freeze for future use.
[0079] (2) Add ethanol with a volume fraction of 90% to the dry powder of Sargassum sargassum, and then reflux for extraction for about 2 hours. After the reflux, filter out the ethanol, then place the Sargassum sargassum powder in a fume hood to completely volatilize the ethanol, and finally dry the Sargassum sargassum powder in a drying oven at a drying temperature of 20°C until it reaches a constant weight. .
[0080] (3) get dry degrea...
Embodiment 3
[0093] The preparation of embodiment 3 Sargassum herbaceous polysaccharide extract and Sargassum herbaceous polyphenol extract (three)
[0094] 1. Method steps
[0095] (1) Remove impurities from the raw material Sargassum sargassum and wash it with water, put the cleaned Sargassum sargassum into a drying box, dry at 40°C for 12 hours to constant weight, and then put the dried Sargassum sargassum in Pulverize in a pulverizer to obtain powder, pass through a 10-mesh sieve to obtain dry powder of Sargassum pratense, and freeze for future use.
[0096] (2) Add ethanol with a volume fraction of 70% to the dry powder of Sargassum sargassum, and then reflux for extraction for about 4 hours. After the reflux, filter out the ethanol, then place the Sargassum sargassum powder in a fume hood to completely volatilize the ethanol, and finally dry the Sargassum sargassum powder in a drying oven at a drying temperature of 40°C until it reaches a constant weight. .
[0097] (3) get dry degr...
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