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Sample testing analysis meter and method for nuclear magnetism analysis

An analyzer and sample technology, applied in the field of sample detection analyzers, can solve the problems of large sample volume, poor sensitivity of nuclear magnetic analysis, and inability to measure

Inactive Publication Date: 2015-08-19
衢州普林千叶电子科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The purpose of the present invention is to overcome the poor sensitivity of nuclear magnetic analysis in the process of detecting and analyzing samples in the prior art, which requires a large amount of samples, and can only measure nuclei with high natural abundance, but cannot detect nuclei with low abundance. Defects of determination, thereby providing a sample detection analyzer and method for nuclear magnetic analysis

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  • Sample testing analysis meter and method for nuclear magnetism analysis
  • Sample testing analysis meter and method for nuclear magnetism analysis
  • Sample testing analysis meter and method for nuclear magnetism analysis

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Embodiment example

[0089] Sample 1:

[0090]

[0091] (4-sulfamoylphenylamino)sodium methanesulfonate is gasified by the gas ionizer and then subjected to high-frequency discharge to ionize the sample gas to generate positive ions in a low charge state; then in the high-frequency electric field of the gas ionizer, the charged The ions collide with the sample atoms and molecules, ionize the sample molecules, and the charged particles multiply to form an infinite discharge, generating a large number of sample charged ions;

[0092] Then the positive booster and the negative booster contained in the ion current generator 2 cooperate to produce positive and negative ions with different charge ratios, and then the ion current generator transmits the positive and negative ions produced to the ion current concentrator through the ion current conduit; The flow concentrator accepts the ion flow from the gas ionizer and the ion flow generator, and then transmits the collected ion flow to the particle m...

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Abstract

The invention discloses a sample testing analysis meter and method for nuclear magnetism analysis. The sample testing analysis meter comprises a gas ionizer, an ion flow generator, an ion flow concentrator, a particle mass filter, an optical lens device, a sample injector, a particle beam controller, an optical signal transduction device, an electric field analyzer, a particle energy analyzer, a signal refractor, a motional magnetic field resolver, a particle conductor, a signal concentrator, a particle electric field controller, a particle channel plate, a fluorescent display screen, a signal observer, a particle camera, a video signal transduction device, a particle multiplier and a computer. The gas ionizer is connected with the ion flow concentrator through a composite conduit made of polyether-ether-ketone chlorobenzene hydrazine. The gas ionizer comprises a high frequency ionization tube; a pipe network coil and M-type electrodes are wound outside the high frequency ionization tube, the pipe network coil is located in the middle outside the high frequency ionization tube, and the M-type electrodes are located at two end parts outside the high frequency ionization tube.

Description

technical field [0001] The invention relates to a sample detection analyzer and method, in particular to a sample detection analyzer and method for nuclear magnetic analysis. Background technique [0002] The principle of sample detection and analysis for nuclear magnetic analysis is based on the physical process of atomic nuclei with a non-zero magnetic moment, Zeeman splitting of the spin level under the action of an external magnetic field, and resonant absorption of radio frequency radiation of a certain frequency. NMR analysis is a branch of spectroscopy, its resonance frequency is in the radio frequency band, and the corresponding transition is the transition of nuclear spin on the nuclear Zeeman energy level. The nuclear magnetic analysis technology used today often adopts CW-NMR analysis technology. Although this technical solution is low in price, high in temperature, and easy to operate, it has poor sensitivity, requires a large amount of sample, and can only measu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N24/08
Inventor 储冬红彭飞
Owner 衢州普林千叶电子科技有限公司