Alfalfa leaf extract preparation method and use as tobacco product additive

A technology of leaf extract and alfalfa is applied in the directions of preparing tobacco, tobacco, processing tobacco, etc., can solve the problems of inability to meet the requirements for the use of cigarette additives, no literature report on alfalfa extract, etc., and achieves rich aroma and thick feeling. , the effect is obvious

Inactive Publication Date: 2015-09-16
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, at present, alfalfa research is mostly used in agriculture, animal husbandry and medicine, and there is no literature report that alfalfa extract is used as a cigarette additive.
And in the process of our research, we found that the alfalfa extract obtained by simple solvent extraction has a relatively large negative effect and cannot meet the requirements for use as a cigarette additive

Method used

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  • Alfalfa leaf extract preparation method and use as tobacco product additive

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Firstly, phenylacetic acid is added to 75% ethanol aqueous solution by volume fraction, the pH value of ethanol aqueous solution is 5.0, the volume ratio of ethanol aqueous solution and alfalfa leaf is 30:1, extract at 90° C. for 3 hours, and after separating the primary feed liquid, add it to the primary feed Add 2 times the volume of water (sodium carbonate is added to adjust the pH value to 8.5) and separate the precipitate. The separated secondary feed liquid is concentrated to the extract with a density of 1.100. The volume fraction of the extract with 8 times the volume is 75 % of ethanol aqueous solution, filter again to separate the by-products and the three feed liquids, and concentrate the three feed liquids again to extract-like, that is, the alfalfa leaf extract 1 of the present invention is obtained.

Embodiment 2

[0027] First add citric acid to 75% ethanol aqueous solution by volume fraction, adjust the pH value of ethanol aqueous solution to 5.5, and the volume ratio of ethanol aqueous solution to alfalfa leaves is 15:1, extract at 50°C for 4 hours, separate the feed liquid once, and feed it once Add 4 times the volume of water to the feed solution (adding ammonia water to adjust the pH value to 9.5) and separate the precipitate. The separated secondary feed solution is concentrated to an extract with a density of 1.300. The volume fraction of the extract with 8 times the volume is 75 % of ethanol aqueous solution, filter again to separate the by-products and the third feeding liquid, and concentrate the third feeding liquid again to the extract form, that is, the alfalfa leaf extract 2 of the present invention is obtained.

Embodiment 3

[0029] First add malic acid to 75% ethanol aqueous solution by volume fraction, adjust the pH value of ethanol aqueous solution to 4.5, the volume ratio of ethanol aqueous solution to alfalfa leaf is 20:1, extract at 60°C for 2 hours, separate the feed liquid once, and feed it once Add 5 times the volume of water to the feed solution (sodium hydroxide is added to adjust the pH value to 10.0) and separate the precipitate. The separated secondary feed solution is concentrated to an extract with a density of 1.200. Use 5 times the volume of the extract in the volume fraction Redissolve in 75% ethanol aqueous solution, filter again to separate the by-products and the third feeding liquid, and concentrate the third feeding liquid again to the extract form to obtain the alfalfa leaf extract 3 of the present invention.

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Abstract

The invention discloses an alfalfa leaf extract preparation method and a use as a tobacco product additive. The method comprises the steps of using alfalfa leaves as extraction raw materials, and uniformly mixing alfalfa leaves with extracting agent according to volume ratio of 1:(10-30) to obtain mixture; extracting the mixture for 1-5h at 50-90DEG C and performing separation to obtain primary material liquid; adding water into the material liquid, separating sediment, performing separation to obtain secondary material liquid and concentrating the secondary material liquid to extract; redissolving the extract by using 5-10 multiples of extracting solution, filtering and separating byproducts and tertiary material liquid, and concentrating the tertiary material liquid to extract to obtain alfalfa leaf extract. By adding the alfalfa leaf extract prepared by adopting the method disclosed by the invention into tobacco products, an effect of effectively increasing the flavor of the tobacco products is achieved, the flavor is rich and the solidity of smoke is increased; the extract can also endow the tobacco products with unique flavor tones and notes, and can be used as a characteristic flavor.

Description

technical field [0001] The invention relates to the application of a natural plant extract in tobacco products, in particular to a preparation method of alfalfa leaf extract and its use as an additive of tobacco products. Background technique [0002] The core competitiveness of "Chinese-style cigarettes" is to form a characteristic style of products, reflect individualization and differentiation, and adapt to the smoking habits and consumption needs of Chinese consumers. Flavors and fragrances for Chinese-style cigarettes are the "soul" of Chinese-style cigarette products and the mystery of the formation of the style and characteristics of "Chinese-style cigarettes". Scientifically adding flavors and ingredients to cigarettes is an important means to highlight the individual style of cigarette products. At the same time, in order to improve the safety of smoking, harm reduction and coke reduction have become an important part of "Chinese cigarettes". While reducing cigare...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/26A24B3/12
CPCA24B15/26A24B3/12
Inventor 谭烨邵兴伟吴昭刘吟肜霖黄龙
Owner HUBEI CHINA TOBACCO IND
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