Comfort spandex fiber and preparation method thereof
A spandex fiber, comfortable technology, applied in the field of functional chemical fiber and its manufacturing, to achieve the effect of saving oil removal process, low modulus, and sufficient separation
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[0023] Step 1: Prepare mixed prepolymer solution
[0024] 1) Prepare a prepolymer solution containing polyether polyol structural units: prepolymerize at 90° C. for 90 minutes with the molar ratio of diisocyanate and polytetrahydrofuran diol at 1.7, and add N to the prepolymer after the prepolymerization is completed, N-dimethylacetamide solvent is made into the prepolymer solution that mass percent concentration is 50%;
[0025] 2) Prepare a prepolymer solution containing dihydroxysilicone oil structural units: prepolymerize at 95°C for 100 min with the molar ratio of diisocyanate to dihydroxysilicone oil at 1.7, and add N,N- The dimethylacetamide solvent is prepared into a prepolymer solution with a concentration of 50% by mass; wherein the relative molecular weight of the dihydroxy silicone oil is 2500.
[0026] 3) Prepare a mixed prepolymer solution: blend the prepolymer solution of step 1) and step 2) at 40° C. for 35 minutes to prepare a mixed prepolymer solution;
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