A kind of preparation method of tungsten-copper-tin alloy powder
A tin alloy and tungsten-copper technology is applied in the field of preparation of tungsten-copper-tin alloy powder, which can solve problems such as easy segregation, and achieve the effects of easy segregation, excellent flow performance and simple preparation process.
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Embodiment 1
[0029] 1) In terms of weight percentage, weigh 80% crystalline tungsten powder, 16% atomized copper powder and 4% tin powder. Among them, the mesh of crystalline tungsten powder is 400 mesh, and the mesh of tin powder is 600 mesh. The mesh number of copper powder is 400 meshes, and the purity of crystalline tungsten powder, tin powder and atomized copper powder is greater than 99.5%;
[0030] 2) Add crystalline tungsten powder, atomized copper powder, and tin powder to w-20 double cone mixer and mix for 30 minutes;
[0031] 3) Take out the material, pass it through the HYL-375-7Q steel belt reduction furnace for high-temperature diffusion in protective gas or reducing atmosphere, set the temperature to 950 degrees Celsius, and the diffusion time to 5h. Through the tin powder in the copper and in the Diffusion in tungsten to realize the alloy connection of copper and tungsten;
[0032] 4) After being out of the furnace, it is crushed and screened by a crusher to obtain tungsten-coppe...
Embodiment 2
[0038] 1) In terms of weight percentage, weigh 60% crystalline tungsten powder, 37% atomized copper powder and 3% tin powder. Among them, the mesh of crystalline tungsten powder is 500 mesh, and the mesh of tin powder is 650 mesh, atomized The mesh number of copper powder is 380 meshes, and the purity of crystalline tungsten powder, tin powder and atomized copper powder is greater than 99.5%;
[0039] 2) Add crystalline tungsten powder, atomized copper powder, and tin powder to w-20 double cone mixer and mix for 30 minutes;
[0040] 3) Take out the material, pass through the HYL-375-7Q steel belt-type reduction furnace for high-temperature diffusion in protective gas or reducing atmosphere, set the temperature to 800 degrees Celsius, and the diffusion time to 4h. Through the tin powder in the copper and in the Diffusion in tungsten to realize the alloy connection of copper and tungsten;
[0041] 4) After being out of the furnace, it is crushed and screened by a crusher to obtain tun...
Embodiment 3
[0046] 1) In terms of weight percentage, weigh 40% crystalline tungsten powder, 58% atomized copper powder and 2% tin powder. Among them, the mesh of crystalline tungsten powder is 600 mesh, and the mesh of tin powder is 600 mesh, atomized The mesh number of copper powder is 400 meshes, and the purity of crystalline tungsten powder, tin powder and atomized copper powder is greater than 99.5%;
[0047] 2) Add crystalline tungsten powder, atomized copper powder, and tin powder to the w-20 double cone mixer and mix for 30 minutes;
[0048] 3) Take out the material, pass it through the HYL-375-7Q steel belt reduction furnace for high-temperature diffusion in protective gas or reducing atmosphere, set the temperature to 750 degrees Celsius, and the diffusion time to 3h. Through the tin powder in the copper and in the Diffusion in tungsten to realize the alloy connection of copper and tungsten;
[0049] 4) After being out of the furnace, it is crushed and screened by a crusher to obtain t...
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