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33results about How to "Hypoxic" patented technology

Rare earth magnesium-alloy material for 3D printing and preparation method of same

The invention belongs to the technical field of 3D printing materials and discloses a rare earth magnesium-alloy material for 3D printing and a preparation method of the same. The preparation method particularly comprises following steps: (1) weighing raw materials according to element mass ratio of Mg:Mn:Re being 85-97:2-10:1-5; (2) adding pure magnesium, pure manganese and magnesium alloy into a pre-heated crucible, adding a cover agent and smelting the mixture under atmospheric conditions; (3) after the mixture smelted completely, adding an Mg-Re intermediate alloy and pure rare earth elements, melting the components with stirring uniformly and increasing the temperature to 700-750 DEG C; (4) adding a refining agent for refining the alloy for 2-25 min, allowing the refined alloy to stand, removing floated slag, adding the refined alloy into a sand mould trough to obtain a rare earth magnesium alloy base metal; and (5) smelting and atomizing the base metal to obtain the rare earth magnesium-alloy material. The rare earth magnesium-alloy material is excellent in flame retarding performance, is easy to control in powder shape and particle size, can be smelted without protective gas so that a problem of flammability during preparation of the magnesium alloy powder through an atomization method is solved, and can be used for laser 3D printing.
Owner:SOUTH CHINA INST OF COLLABORATIVE INNOVATION

Production of pre-reduced chrome ore pellet by external heated shaft furnace

InactiveCN101418372AOvercome the difficulty of controlling the reducing atmosphereOvercome Kiln DifficultiesVertical furnacesCombustion chamberHigh carbon
The invention discloses a chrome ore prereduction external heating type shaft furnace, which is characterized in that multilayer gas burner flame paths arranged on both sides of reduction reaction chambers with a rectangular cross section indirectly supply heat under the condition of air separation. The shaft furnace consists of a plurality of independently working reaction reduction chambers; the reduction reaction chambers and the gas burner flame paths are built by tailored high aluminium special-form refractory bricks; and the shaft furnace body is vertically arranged on a bearing girder. Dried carbon-contained chrome ore pellets are added into a bin on the top end of the shaft furnace and are discharged out of the furnace through the preheating section, the reduction section and the cooling section of the shaft furnace. The temperature of the reduction reaction is 1,300 to 1,400 DEG C; the material stays at the reduction section for 3 to 4 hours; and the comprehensive reduction degree is 60 to 70 percent. The prereduced pellet ore is used for producing high carbon ferrochrome in a closed electric furnace. The cold pellet ore which is charged into the closed electric furnace can reduce the power consumption for ferrochrome by above 25 percent, improve the yield by above 40 percent, reduce the emission by above 20 percent, and improve the chrome recovery rate by above 3 percent. The chrome ore prereduction external heating type shaft furnace can be used for continuous production, and has the advantages of circulation, high economical efficiency, environmental protection, energy conservation, emission reduction, and the like.
Owner:李志忠

Preparation method of high-heat-conduction aluminum nitride thick film

The invention relates to a preparation method of a high-heat-conduction aluminum nitride thick film, belongs to the technical field of surface coating preparation and application and mainly solves the technical problems that an aluminum nitride thick film can not be prepared, the deposition speed is low, commercialization is difficult to realize and the like in the prior art. According to the method, the aluminum nitride thick film is deposited through arc ion plating, the nitrogen/aluminum ratio in the film is uniform, the thickness of the prepared AlN high-heat-conduction film can be up to 3-10mu m, and a large bonding force can be generated between the film and a substrate, wherein the involved substrate material can be metal such as stainless steel, iron, copper, aluminum and the like, or can be an inorganic non-metal material such as ceramic, glass and the like, or can be a high-molecular organic polymer such as epoxy resin, polyimide and the like. The preparation method comprises the following steps: performing surface treatment on the substrate material; and by selecting pure aluminum as a cathode target material and using pure nitrogen gas as reacting gas, forming the AlN high-heat-conduction film through reaction between aluminum ions obtained by ionization and the nitrogen gas, wherein the purity of the aluminum target material is 99.99%, and the purity of the nitrogen gas is 99.999%. Thus, the method is applicable to multiple fields such as electronic measuring instruments, computer equipment, measurement and control systems, airplanes, precision weapons and the like.
Owner:辽宁法库陶瓷工程技术研究中心

Novel preparation technology for mixture taking water as grinding medium

The invention relates to novel preparation technology for a mixture taking water as a grinding medium. The novel preparation technology contains working procedures such as batching, wet grinding, unloading, slurry drying and the like, wherein in the working procedure of the wet grinding, distilled water is adopted as the grinding medium, and 2 to 3 percent of antioxidant substance is added into the distilled water; in the working procedure of unloading, the mixture is unloaded from a wet grinder and passes through a 320-mesh sieve, and the wet grinder is washed for 6 times by water; and in the working procedure of slurry drying, an open type spray drying tower is adopted for drying, slurry is output to a nozzle for atomization by a pump, fog drops move from the bottom up, encounter the hot air which moves from the top down, and then are dried and a material flows out of the tower and is loaded into a material barrel after the automatic cooling. The preparation technology can effectively eliminate potential safety hazard, and save a large amount of energy sources; and the preparation technology does not need fire prevention and explosion prevention, adopts open type spray drying equipment, saves one half of equipment investment, does not need chilled water and nitrogen, and greatly reduces the cost for production operation.
Owner:OKE PRECISION CUTTING TOOLS CO LTD

Preparation method of lithium titanate material

The invention belongs to a lithium battery material, and concretely relates to a preparation method of a lithium titanate material. The method comprises the following steps: 1, adding tetrabutyl titanate into anhydrous ethanol, and uniformly stirring to form a titanium alcohol solution; 2, adding lithium acetate into the titanium alcohol solution, and uniformly stirring to form a mixed solution; 3, adding titanium monoxide powder into the mixed solution, and carrying out low-temperature ultrasonic treatment for 1-2 h to obtain a suspension; 4, spraying the suspension into a constant-temperature reaction kettle, sealing, depositing, decompressing and cooling to obtain coated titanium monoxide particles; and 5, putting the coated titanium monoxide particles into the sealed reaction kettle, carrying out constant-pressure standing for 1-3 h, then introducing water vapor, carrying out a sealed pressurization reaction for 2-3 h, relieving the pressure, and carrying out sealed sintering so asto obtain lithium titanate particles. The problem that an existing lithium titanate material is poor in electrical conductivity is solved; and titanium monoxide is used as an inner core, and lithiumtitanate is used as a surface coating layer, so it is guaranteed that the prepared material has oxygen deficiency, the mobility of electrons is improved, and the electrical conductivity is improved.
Owner:江苏众钠能源科技有限公司

Flue gas secondary re-burning tunnel kiln and flue gas secondary re-burning method

The invention discloses a structure of a flue gas secondary re-burning tunnel kiln and a flue gas secondary re-burning method. The structure is characterized in that a first air cabinet for air inletis installed in a drying room of the tunnel kiln, the first air cabinet is connected to a first centrifugal fan, the first centrifugal fan is connected with first air ducts used for air outlet, the first air ducts are distributed on channels arranged on the two sides of a simplified house, and air outlets of the first air ducts are aligned with a brick pile in the simplified house; and a second air cabinet for air inlet is installed at the upper part of the simplified house, the second air cabinet is connected to a second centrifugal fan, the second centrifugal fan is connected with second airducts used for air outlet, and the second air ducts are arranged on the two sides in a roasting channel low-temperature section of a roasting channel. According to the flue gas secondary re-burning tunnel kiln, the waste heat of finished bricks is fully utilized, the waste heat is used for baking the flue gas coming out of the drying room, the roasting channel is injected with the dry flue gas ofhot air, so that the roasting channel is not cooled, the roasting channel is fast to roast, the finished brick is fast to produce, and the problems of high coal consumption, poor product quality, lowyield and high oxygen content are effectively prevented.
Owner:江西振大机械制造科技有限公司

A rare earth magnesium alloy material for 3D printing and its preparation method

The invention belongs to the technical field of 3D printing materials and discloses a rare earth magnesium-alloy material for 3D printing and a preparation method of the same. The preparation method particularly comprises following steps: (1) weighing raw materials according to element mass ratio of Mg:Mn:Re being 85-97:2-10:1-5; (2) adding pure magnesium, pure manganese and magnesium alloy into a pre-heated crucible, adding a cover agent and smelting the mixture under atmospheric conditions; (3) after the mixture smelted completely, adding an Mg-Re intermediate alloy and pure rare earth elements, melting the components with stirring uniformly and increasing the temperature to 700-750 DEG C; (4) adding a refining agent for refining the alloy for 2-25 min, allowing the refined alloy to stand, removing floated slag, adding the refined alloy into a sand mould trough to obtain a rare earth magnesium alloy base metal; and (5) smelting and atomizing the base metal to obtain the rare earth magnesium-alloy material. The rare earth magnesium-alloy material is excellent in flame retarding performance, is easy to control in powder shape and particle size, can be smelted without protective gas so that a problem of flammability during preparation of the magnesium alloy powder through an atomization method is solved, and can be used for laser 3D printing.
Owner:SOUTH CHINA INST OF COLLABORATIVE INNOVATION

Preparation method of aluminum nitride thick film with high heat conductivity and high heat dissipation properties

The invention discloses a preparation method of an aluminum nitride thick film with high heat conductivity and high heat dissipation properties. In the method, pure aluminum is selected as a cathode target, the purity of the aluminum target is 99.99%, pure nitrogen is adopted as reaction gas, the purity of nitrogen is 99.999%, and aluminum ions obtained through ionization react with nitrogen to form an A1N high-heat-conductivity film. The method comprises the implementation steps that 1, a workpiece substrate is cleaned, dried and placed into a sample chamber, vacuum pumping is carried out, and the vacuum degree needs to be controlled below 9*10<-3>Pa in order to obtain a high-quality aluminum nitride coating; 2, high-purity Ar gas is led in for carrying out sputtering cleaning; 3, argon leading, arc starting, negative bias adding and nitrogen leading are carried out, nitrogen pressure is 1-3*10<-1>Pa, and pre-bombardment cleaning is carried out under the negative bias of 250 V-650 V for 10-180 min. The aluminum nitride thick film can be deposited on the surface of a complex sample, and the film layer preparation method is most widely applied to the engineering technical field. Themethod is simple, operation is easy, the technology is practical, and the method is suitable for industrial production. The prepared aluminum nitride thick film is uniform in ratio, low in nitrogen content and high in heat conductivity.
Owner:辽宁法库陶瓷工程技术研究中心

A kind of preparation method of lithium titanate material

The invention belongs to lithium battery materials, and specifically relates to a method for preparing a lithium titanate material, comprising the following steps: step 1, adding tetrabutyl titanate into absolute ethanol and stirring evenly to form a titanium alcohol solution; step 2, adding acetic acid Lithium is added to the titanic acid solution and stirred evenly to form a mixed solution; step 3, the titanium monoxide powder is added to the mixed solution by low-temperature ultrasound for 1-2 h to obtain a suspension; step 4, the suspension is sprayed to the constant temperature reaction kettle In the process, the coated titanium monoxide particles are obtained after sealing deposition and pressure relief cooling; step 5, the coated titanium monoxide particles are placed in the sealed reaction kettle for 1-3 hours under constant pressure, and then water vapor is introduced to carry out the sealed and pressurized reaction 2- 3h, after the pressure was released, it was sealed and sintered to obtain lithium titanate particles. The invention solves the problem of poor electrical conductivity of the existing lithium titanate material, uses titanium monoxide as the inner core, and uses lithium titanate as the surface coating layer to ensure that the prepared material has oxygen deficiency, improves the mobility of electrons, and thus improves the the conductivity.
Owner:江苏众钠能源科技有限公司

Anti-deterioration storage method of frozen food

The invention discloses an anti-deterioration storage method of frozen food. The anti-deterioration storage method comprises the following steps: spraying a trehalose solution to the surface of the to-be-frozen food; wherein the spraying amount is 0.2-0.4% of the weight of the to-be-frozen food, then putting the frozen food sprayed with the trehalose solution into a closed pressure bin, applying pressure for 1-2 h at the pressure of 80-120 Mpa, and then performing ventilation and airing under the room temperature condition to enable the moisture content of the frozen food to be not higher than4% for standby application; performing vacuumizing; performing bag opening packaging on the frozen food obtained after degassing treatment is completed; and freezing and storing, namely storing the packaged frozen food in a refrigeration house; according to the anti-deterioration storage method of the frozen food, surface treatment, vacuumizing, packaging and freezing storage are conducted on theto-be-frozen food, the fresh-keeping rate of the food can be achieved to the maximum extent, the expiration date of the food is guaranteed to the maximum extent, and therefore the expiration time ofthe food is shortened, the practical time of the food is prolonged, and practicability is achieved.
Owner:江苏丰诺供应链管理集团有限公司

Novel preparation technology for mixture taking water as grinding medium

The invention relates to novel preparation technology for a mixture taking water as a grinding medium. The novel preparation technology contains working procedures such as batching, wet grinding, unloading, slurry drying and the like, wherein in the working procedure of the wet grinding, distilled water is adopted as the grinding medium, and 2 to 3 percent of antioxidant substance is added into the distilled water; in the working procedure of unloading, the mixture is unloaded from a wet grinder and passes through a 320-mesh sieve, and the wet grinder is washed for 6 times by water; and in the working procedure of slurry drying, an open type spray drying tower is adopted for drying, slurry is output to a nozzle for atomization by a pump, fog drops move from the bottom up, encounter the hot air which moves from the top down, and then are dried and a material flows out of the tower and is loaded into a material barrel after the automatic cooling. The preparation technology can effectively eliminate potential safety hazard, and save a large amount of energy sources; and the preparation technology does not need fire prevention and explosion prevention, adopts open type spray drying equipment, saves one half of equipment investment, does not need chilled water and nitrogen, and greatly reduces the cost for production operation.
Owner:OKE PRECISION CUTTING TOOLS CO LTD

A preparation method, material and application of 3D printing medical magnesium alloy material

The invention discloses a preparing method, material and application of a medical magnesium alloy material used for 3D printing. The magnesium alloy material comprises, by mass, 10-16wt% of Fe, 1-3wt% of Mn, 0.2-2wt% of Zn, 0.5-3wt% of Ca and the balance Mg. According to the preparing steps, the material is prepared according to the compositions and the mass; pure magnesium, pure manganese, pure zinc and pure calcium are put into a preheated crucible, a covering agent is added, and the mixed material is smelted on the atmosphere condition; after the mixed material is smelted, a magnesium iron intermediate alloy is added, after the mixed material is smelted, the mixed material is stirred uniformly, and the temperature is stabilized to range from 700 DEG C to 740 DEG C; a refining agent is added, refining is carried out for 5-30 min, the material stands for 10-30 min at the temperature of 700 DEG C-740 DEG C, surface dross is skimmed, the material is poured into a metal mould, and medical magnesium alloy base metal is obtained; and the base metal is smelted and atomized, and the medical magnesium alloy material is obtained. The medical magnesium alloy material is a multi-element degradable alloy material completely composed of biosecurity human body nutrient elements, has an excellent flame retardant property, can degrade an inner implanted material medically, has an important application potential in the 3D printing field, and has a good application prospect, and the powder shape and the particle diameter are easy to control.
Owner:苏州轻金三维科技有限公司
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