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A short-time dipping flax degumming process

A flax and degumming technology, which is applied in the direction of producing bast fiber by chemical method, can solve the problem of high production cost of enzymatic degumming, and achieve the effect of meeting environmental protection, reducing consumption and saving production cost

Active Publication Date: 2018-04-13
QIQIHAR UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the basis of enzymatic degumming, the short-time impregnation process can reduce the amount of enzyme preparation, thereby solving the problem of high production cost of enzymatic degumming, and is conducive to promoting the industrial production of enzymatic degumming

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Harvested raw flax stems were processed with a roller compactor to break the epidermis, rinsed with water, and soaked in water for 9 hours at a water bath ratio of 1:20 (w / v). Put the pretreated raw flax stems in water, soak for 20 minutes, and drench for 1 minute to remove excess water. The measured water consumption is 33.4%. Insulate at 30°C for degumming. After 96 hours, the degumming was completed. Rinse with water repeatedly to remove the degumming solution, and heat and dry at 80°C to obtain flax fibers.

[0019] The control experiment carried out at the same time did not adopt the short-time dipping process, and the degumming completion time was 96 hours.

Embodiment 2

[0021] Harvested raw flax stems were washed with water and soaked in water for 10 hours at a water bath ratio of 1:20 (w / v). The pretreated raw flax stems were placed in 4 g / L alkaline pectinase enzyme preparation solution added with 0.2% ammonium oxalate, soaked for 10 minutes, and drenched for 30 seconds, and the consumption of enzyme solution was measured to be 26.7%. Insulated at 45°C for degumming. After 48 hours, the degumming was completed. Rinse repeatedly with water to remove the enzyme solution, heat and dry at 80°C to obtain flax fibers.

[0022] The control experiment carried out at the same time did not adopt the short-time dipping process, and the degumming completion time was 40 hours.

Embodiment 3

[0024] Harvested raw flax stems were washed with water and soaked in water for 10 hours at a water bath ratio of 1:20 (w / v). The pretreated flax raw stems were placed in water added with 2g / L urea, soaked for 30 minutes, and drenched for 30 seconds. The consumption of urea aqueous solution was measured to be 28.4%. Insulate at 35°C for degumming. After 100 hours, the degumming was completed. Rinse repeatedly with water to remove the degumming solution, and heat and dry at 100°C to obtain flax fibers.

[0025] The control experiment carried out at the same time did not adopt the short-time dipping process, and the degumming completion time was 96 hours.

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Abstract

The invention relates to a new process of degumming flax by soaking for a short time, and relates to the technical field of flax degumming. In the present invention, the pretreated raw flax stems are soaked in the degumming solution for a short time, and after taking out and drenching excess degumming solution, the degumming is carried out with heat preservation. After the degumming is completed, the flax fibers are obtained by washing with water and drying. The short-time dipping process of the present invention can reduce the amount of degumming solution by 70%. For the current degumming method of flax by soaking in warm water, it can greatly reduce the water pollution and air pollution caused by the discharge of retting waste liquid; it is applied to the promising enzymatic degumming method, and the composition and structure of the enzymatic degumming fiber can be controlled. On the basis of the advantages of mild action conditions, etc., because the amount of enzyme solution is reduced, the problem of high cost of enzyme preparations that restricts the industrial application of enzymatic degumming can be solved. The short-time impregnated flax degumming process of the present invention has the advantages of simple process, low production cost, environmental friendliness and high degumming efficiency.

Description

technical field [0001] The invention relates to the field of flax degumming, in particular to a short-time dipping flax degumming process. Background technique [0002] Known as the "fiber queen", flax is a high-quality natural plant fiber. The history of being used by humans for textiles can be traced back to ancient Egypt. Linen fabric has excellent characteristics such as fast moisture absorption and heat dissipation, good air permeability, antibacterial and antiseptic, and antistatic. To obtain spinnable flax fiber, it must be degummed. Degumming refers to the destruction of the glue that connects the bast fiber bundles with the surrounding tissue, so that the flax fibers located in the phloem are separated from the xylem, and non-cellulose substances (such as: pectin, hemicellulose and lignin, etc.) Silky mature flax fibers. Degumming is a key link in flax processing, and the degumming effect directly affects the subsequent flax processing processes such as beating a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01C1/02
Inventor 刘晓兰王路田英华郑喜群
Owner QIQIHAR UNIVERSITY