Traditional Chinese medicine composition for treating urinary calculi and preparation method thereof
A technique for urinary calculus and composition, which is applied in the field of traditional Chinese medicine composition for treating urinary calculus and its preparation, and can solve problems such as unsatisfactory treatment effect of traditional Chinese medicine, large toxic and side effects of western medicine, and difficulty in sustaining the therapeutic effect.
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[0046] The present invention also provides a preparation method of the above-mentioned traditional Chinese medicine composition, including:
[0047] The ingredients in the raw material components are mixed in proportion, crushed, soaked in 4-6 times the amount of water for 12-24 hours, and the volatile oil is extracted by steam distillation. The slag and liquid after distillation are stored separately, and the liquid is reduced. The relative density is 1.14-1.21 at 65-75℃ to obtain A; the above-mentioned volatile oil is dissolved by adding 65% ethanol at a ratio of 1:1, using colloid milling method, and the ratio of volatile oil to β-cyclodextrin is 1:5 -8, The ratio of β-cyclodextrin to water is 1:1-4, and the inclusion compound is obtained by grinding at an appropriate grinding speed for 15-30 minutes to obtain a paste, which is dried at 55-65°C and crushed to obtain an inclusion compound B; The above-mentioned drug residue is continued to be refluxed with 65-75% ethanol for 1-...
Embodiment 1
[0052] Take 10 parts by weight of Achyranthes bidentata, 8 parts by weight of thistle, 6 parts by weight of green bark, 8 parts by weight of Cyperus rotundus, 5 parts by weight of Gallus gallus domesticus, 10 parts by weight of Morinda officinalis, 9 parts by weight of Triangle, 6 parts by weight of honeysuckle, 5 parts by weight of Xu Changqing, 6 parts by weight of magnet, 8 parts by weight of Houttuynia cordata, 8 parts by weight of hawthorn, 10 parts by weight of ginkgo, 6 parts by weight of Citrus aurantium, 5 parts by weight of myrrh, mixed in proportion and crushed; 4 times the amount of water Soak for 12 hours, extract the volatile oil by steam distillation, save the distilled medicine residue and medicine solution separately, and recover the medicine solution under reduced pressure and concentrate to a relative density of 1.14 at 65°C to obtain A; add 65% ethanol to the above volatile oil at a ratio of 1:1 Dissolve, use colloid milling method, make the ratio of volatile...
Embodiment 2
[0056] Take 16 parts by weight of Achyranthes bidentata, 14 parts by weight of thistle, 12 parts by weight of green bark, 15 parts by weight of Cyperus rotundus, 10 parts by weight of Gallus gallus domesticus, 16 parts by weight of Morinda officinalis, 18 parts by weight of triangular ribs, and 14 parts by weight of honeysuckle vine, 10 parts by weight of Xu Changqing, 12 parts by weight of magnets, 18 parts by weight of Houttuynia cordata, 14 parts by weight of hawthorn, 16 parts by weight of ginkgo, 12 parts by weight of citrus aurantium, 10 parts by weight of myrrh, mixed in proportion and crushed; use 6 times the amount of water Soak for 24 hours, extract the volatile oil by steam distillation, save the distilled medicine residue and medicine solution separately, and recover the medicine solution under reduced pressure and concentrate to a relative density of 1.21 at 75℃ to obtain A; add 65% ethanol to the above volatile oil at a ratio of 1:1 Dissolve, use the colloid mill m...
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