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Nanometer micro-emulsion composition, preparation method thereof and application of nanometer micro-emulsion composition to cosmetic

A technology of microemulsion and composition, which is applied in the field of nano microemulsion composition and its preparation and application in cosmetics, can solve the problem of limited application range of gel emulsification method, difficulty in obtaining clear and transparent materials, product safety and Stickiness problem and other problems, to achieve the effect of not easy to delaminate, easy to absorb, and improve stability

Inactive Publication Date: 2015-12-09
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The traditional cosmetic emulsification process often uses physical, chemical and mechanical methods to prepare O / W or W / O emulsions, but due to the different polarity of the water-oil system, such emulsions often show low heat-resistant or cold-resistant stability
For example: the emulsification particles produced by the phase inversion emulsification method are large, which makes the product easy to layer; the HLB temperature emulsification method is extremely sensitive to temperature and water-oil ratio, and it is difficult to obtain a clear and transparent material body when used in makeup water; the gel emulsification method The scope of application is limited and it is difficult to be widely used; the liquid crystal emulsification method has strict requirements on surfactants in order to form the required microcrystalline phase
[0003] Transparent or translucent nano-microemulsion composition is a type of composition with a particle size between 10 and 100nm. Due to the high content of surfactants in the previous formulations and the safety and stickiness of the product, etc. problems, so that it has not been widely used in cosmetics

Method used

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  • Nanometer micro-emulsion composition, preparation method thereof and application of nanometer micro-emulsion composition to cosmetic

Examples

Experimental program
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Effect test

Embodiment 1

[0044] A kind of preparation of nano microemulsion composition:

[0045] Mix 11.2 parts by weight of surfactant (cocamidopropyl betaine) and 27.5 parts by weight of oil phase (isomeric hexadecane), and heat up to completely dissolve at 80°C to obtain a mixed system; slowly mix 27 parts by weight 34.3 parts by weight of deionized water are heated up to 80°C, and the surfactant, oil phase, The glycerin mixture was added into deionized water, stirred at a speed of 38 rpm until clear and transparent, and cooled to obtain a nano-microemulsion composition. The viscosity of the prepared composition is 3870mPa·s; the particle size of the particles is 10-100nm.

Embodiment 2

[0047] A kind of preparation of nano microemulsion composition:

[0048]20 parts by weight of the surfactant (14 parts by weight of polyglycerol fatty acid ester and 6 parts by weight of laurate) and 10 parts by weight of the oil phase (jojoba oil) are heated to completely dissolve at 80 ° C; slowly 30 parts by weight Parts by weight of glycerin are heated to 80°C, and added to polyglycerol fatty acid ester, laurate and jojoba oil to obtain a mixture; 40 parts by weight of deionized water is raised to 80°C, and the surfactant, oil phase The mixture of glycerin and glycerin was added into deionized water, stirred at a speed of 35 rpm until clear and transparent, and cooled to obtain a nano-microemulsion composition. The viscosity of the prepared composition is 4250mPa·s; the particle size of the particles is 10-100nm.

Embodiment 3

[0050] A kind of preparation of nano microemulsion composition:

[0051] Heat 1 part by weight of surfactant (hydrogenated castor oil) and 0.1 part by weight of oil phase (macadamia nut oil) at 75°C until completely dissolved; slowly raise the temperature of 0.5 part by weight of glycerin to 75°C, and add to hydrogenated castor oil and macadamia nut oil to obtain a mixture; heat up 40 parts by weight of deionized water to 80°C, slowly add the mixture of surfactant, oil phase and glycerin to deionized water, and stir at a speed of 30 rpm until clear and transparent , cooling down to obtain the nano microemulsion composition. The viscosity of the prepared composition is 1550mPa·s; the particle size of the particles is 10-100nm.

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Abstract

The invention discloses a nanometer micro-emulsion composition, preparation thereof and application of the nanometer micro-emulsion composition to a cosmetic. The nanometer micro-emulsion composition is mainly prepared from a main surfactant, an oil phase component, glycerinum and an aqueous phase component, wherein the main surfactant is at least one of poly(propylene glycol) fatty acid ester, hydrogenated castor oil and polyglycerol fatty acid ester, the oil phase component is at least one of macadamia oil, jojoba oil, isohexadecane and olive oil, and the aqueous phase component is deionized water. The nanometer micro-emulsion composition is smaller in particle diameter, uniform in particle size, better in stability and low in layering possibility, a preparation method is simple, and technological parameters are relatively flexible and can be correspondingly adjusted according to material difference; besides, the nanometer micro-emulsion composition is used in the cosmetic field, can obviously improve the use feeling of the cosmetic, light skin-touch is realized, the cosmetic is extremely easy to absorb by the skin, and the stability of the cosmetic can be improved.

Description

technical field [0001] The invention relates to an emulsified composition, in particular to a nano-microemulsified composition and its preparation and application in cosmetics. Background technique [0002] The traditional cosmetic emulsification process often uses physical, chemical and mechanical methods to prepare O / W or W / O emulsions, but due to the different polarity of the water-oil system, such emulsions often show low heat-resistant or cold-resistant stability . For example: the emulsification particles produced by the phase inversion emulsification method are large, which makes the product easy to layer; the HLB temperature emulsification method is extremely sensitive to temperature and water-oil ratio, and it is difficult to obtain a clear and transparent material body when used in makeup water; the gel emulsification method The scope of application is limited and it is difficult to be widely used; the liquid crystal emulsification method has strict requirements o...

Claims

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Application Information

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IPC IPC(8): A61K8/92A61K8/86A61K8/34A61K8/31A61Q19/00
CPCA61K8/922A61K8/31A61K8/34A61K8/86A61K2800/413A61Q19/00
Inventor 赵丹东刘宏生王春艳张少波
Owner SOUTH CHINA UNIV OF TECH
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