A kind of composite phosphate inorganic binder for 3D sand printing and preparation method thereof
A composite phosphate and inorganic binder technology, which is applied to casting molding equipment, cores, casting molds, etc., can solve the problems of restricted application, poor moisture absorption resistance, and poor collapsibility, and achieve extended storage and use time and moisture absorption resistance. Excellent, the effect of overcoming poor moisture absorption resistance
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Embodiment 1
[0025] The raw materials of the composite phosphate inorganic binder for 3D sand printing in this embodiment are: aluminum hydroxide 6.5%, magnesium carbonate 3%, boric acid 3%, 85% industrial phosphoric acid 50%, urea 1%, xylitol 2 %, D-sorbitol 2%, citric acid 1%, aluminum tripolyphosphate 2.5%, aluminum dihydrogen tripolyphosphate 4%, deionized water 25%.
[0026] The preparation method of a kind of 3D sand mold printing composite phosphate non-scrupulous binder of the present embodiment is:
[0027] Step 1, add 65Kg aluminum hydroxide and 250Kg deionized water into the enamel reaction kettle, start stirring and start heating to a slight boiling state;
[0028] Step 2: Slowly add 500kg of 85% industrial phosphoric acid. After the reaction is clear and transparent, continue the reaction for at least 1 hour. Turn off the heating. After the temperature drops to 60°C, slowly add 30Kg of magnesium carbonate, and keep the temperature at 60°C for at least 30 minutes. heated to a ...
Embodiment 2
[0033] The raw materials of the composite phosphate inorganic binder for 3D sand printing in this embodiment are: aluminum hydroxide 7%, magnesium carbonate 3%, boric acid 4.5%, 85% industrial phosphoric acid 47%, urea 1%, xylitol 1.5% %, D-sorbitol 1.5%, citric acid 1%, aluminum tripolyphosphate 3%, aluminum dihydrogen tripolyphosphate 3%, deionized water 27.5%.
[0034] The preparation method of a kind of 3D sand mold printing composite phosphate non-scrupulous binder of the present embodiment is:
[0035] Step 1, add 70Kg aluminum hydroxide and 275Kg deionized water into the enamel reaction kettle, start stirring and start heating to a slight boiling state;
[0036] Step 2: Slowly add 470kg of 85% industrial phosphoric acid. After the reaction is clear and transparent, continue the reaction for at least 1 hour, turn off the heating, and when the temperature drops to 60°C, slowly add 30Kg of magnesium carbonate, and keep the temperature at 60°C for at least 30 minutes, and t...
Embodiment 3
[0041] The raw materials of the composite phosphate inorganic binder for 3D sand printing in this embodiment are: aluminum hydroxide 9%, magnesium carbonate 4%, boric acid 6%, 85% industrial phosphoric acid 45%, urea 1.5%, xylitol 2 %, D-sorbitol 2%, citric acid 1.5%, aluminum tripolyphosphate 6%, aluminum dihydrogen tripolyphosphate 6%, deionized water 17%.
[0042] The preparation method of a kind of 3D sand mold printing composite phosphate non-scrupulous binder of the present embodiment is:
[0043] Step 1, add 90Kg aluminum hydroxide and 170Kg deionized water into the enamel reaction kettle, start stirring and start heating to a slight boiling state;
[0044] Step 2: Slowly add 450kg of 85% industrial phosphoric acid. After the reaction is clear and transparent, continue the reaction for at least 1 hour. Turn off the heating. After the temperature drops to 60°C, slowly add 40Kg of magnesium carbonate, and keep the temperature at 60°C for at least 30 minutes. heated to a ...
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