Preparation method of graphene modified slurry heat insulation material

A graphene modification and thermal insulation material technology, applied in the field of building materials, can solve the problems of difficult quality control and assurance, poor crack resistance, poor weather resistance, low construction efficiency, etc., and achieves good elasticity, strong compression resistance, and sound insulation effect. Good results

Inactive Publication Date: 2015-12-23
孟红琳
View PDF10 Cites 8 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] my country's thermal insulation materials are currently in a period of development. Although some gratifying progress has been made, the overall technical level is backward, especially in the research and development of slurry thermal insulation materials.
At present, a large number of slurry thermal insulation materials used in civil engineering in my country are stil

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of a graphene-modified slurry insulation material, comprising the following steps:

[0020] Step 1, in parts by weight, add 4 parts of expanded perlite, 2 parts of polystyrene particles, 1 part of graphene, 3 parts of aluminum silicate fiber, 1 part of lecithin, and 3 parts of glycerol into the mixer, and stir Mix to get mixture A;

[0021] Step 2, in parts by weight, add 10 parts of the mixture A obtained in step 1 to the reaction kettle, heat to 60°C, add 3 parts of phenolic resin and 2 parts of diphenylsilanediol, and stir to obtain the mixture B;

[0022] Step 3, in parts by weight, add 8 parts of the mixture B to the reflux device, add 20 parts of absolute ethanol, heat to reflux, filter, and dry to obtain the mixture C;

[0023] Step 4, in parts by weight, heat 7 parts of the mixture to 40°C under vacuum, add 2 parts of gelatin, 1 part of dibutyltin dilaurate, and 3 parts of n-butyl borate, stir, heat up to 60°C, and stir, Cool to room tempe...

Embodiment 2

[0029] A preparation method of a graphene-modified slurry insulation material, comprising the following steps:

[0030] Step 1, in parts by weight, add 6 parts of expanded perlite, 5 parts of polystyrene particles, 3 parts of graphene, 7 parts of aluminum silicate fiber, 2 parts of lecithin, and 9 parts of glycerol into the mixer, and stir Mix to get mixture A;

[0031] Step 2: In parts by weight, add 14 parts of the mixture A obtained in Step 1 to the reactor, heat to 75°C, add 6 parts of phenolic resin and 4 parts of diphenylsilanediol, and stir to obtain the mixture B;

[0032] Step 3, in parts by weight, add 12 parts of the mixture B to the reflux device, add 26 parts of absolute ethanol, heat to reflux, filter, and dry to obtain the mixture C;

[0033] Step 4, in parts by weight, heat 15 parts of the mixture C to 45°C under vacuum, add 4 parts of gelatin, 2 parts of dibutyltin dilaurate, and 5 parts of n-butyl borate, stir, heat up to 70°C, and stir. Cool to room temper...

Embodiment 3

[0039] A preparation method of a graphene-modified slurry insulation material, comprising the following steps:

[0040] Step 1, in parts by weight, add 8 parts of expanded perlite, 3 parts of polystyrene particles, 4 parts of graphene, 6 parts of aluminum silicate fiber, 2 parts of lecithin, and 11 parts of glycerin into the mixer, and stir Mix to get mixture A;

[0041] Step 2: In parts by weight, add 17 parts of the mixture A obtained in Step 1 to the reactor, heat to 70°C, add 5 parts of phenolic resin and 4 parts of diphenylsilanediol, and stir to obtain the mixture B;

[0042] Step 3, in parts by weight, add 14 parts of the mixture B to the reflux device, add 28 parts of absolute ethanol, heat to reflux, filter, and dry to obtain the mixture C;

[0043] Step 4, in parts by weight, heat 17 parts of the mixture to 55°C under vacuum, add 5 parts of gelatin, 2 parts of dibutyltin dilaurate, and 4 parts of n-butyl borate, stir, heat up to 85°C, and stir. Cool to room tempera...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Flexural strengthaaaaaaaaaa
Login to view more

Abstract

The invention provides a preparation method of a graphene modified slurry heat insulation material. According to the method, firstly, expanded perlite, polystyrene particles, graphene, aluminum silicate fiber, lecithin and glycerol are added into a stirring machine; stirring and mixing are carried out; then, an obtained mixture A is added into a reaction kettle; heating is performed; phenolic resin and diphenyl silanediol are added; then, a mixture B is added into a backflow device; absolute ethyl alcohol is added; heating back flow, filtering and drying are carried out; finally, a mixture C is subjected to temperature rise under the vacuum condition; gelatin, dibutyltin dilaurate and n-butyl borate are added; stirring, temperature rise, stirring and cooling to room temperature are performed, and the graphene modified slurry heat insulation material is obtained. The folding-resistant intensity of the obtained heat insulation material can reach more than 10MPa; the absorption rate is lower than 25 percent; the heat conduction coefficient is higher than 0.08W*(mk)-1.

Description

technical field [0001] The invention belongs to the technical field of building materials, and in particular relates to a preparation method of a graphene-modified slurry thermal insulation material. Background technique [0002] After the 1970s, foreign countries generally paid attention to the production of thermal insulation materials and their application in construction, and strived to greatly reduce energy consumption, thereby reducing environmental pollution and greenhouse effect. The thermal insulation material industry in foreign countries has a long history, and thermal insulation materials for building energy conservation account for the vast majority. Cotton products are used for energy saving in buildings. [0003] Building energy conservation is not only the promulgation and implementation of building energy conservation laws and regulations, but its realization also involves a huge industrial group, among which thermal insulation materials and products are an...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C04B26/12C04B22/02
Inventor 孟红琳
Owner 孟红琳
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap