Technology for producing high-purity aminoacetic acid based on urotropine cyclic utilization technology
A technology of pure aminoacetic acid and urotropine, applied in the production process field of high-purity aminoacetic acid based on urotropine recycling technology, can solve product quality, yield fluctuation, unstable process index control, crystallization temperature Inappropriate and other problems, to achieve the effect of high reuse rate, increase resource utilization rate, increase purity and yield
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[0031] The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only some, not all, embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without creative efforts fall within the protection scope of the present invention.
[0032] Such as figure 1 Shown, the production technology that the present invention proposes based on urotropine recycling technology to produce high-purity aminoacetic acid, comprises
[0033] Follow the steps below:
[0034] Step 1: Add chloroacetic acid and urotropine to the dissolution kettle, then add methanol, heat and dissolve, and keep the temperature at 40°C±2°C to obtain a solution;
[0035] Step 2: Move the solution into the reaction kettle, slowly inj...
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