a nb 3 Preparation method of al superconducting wire precursor
A technology of superconducting wires and precursors, applied in the usage of superconductor elements, cable/conductor manufacturing, superconducting/high-conducting conductors, etc., can solve problems such as core wire coupling and magnetic flux jumping, and reduce AC loss value, The effect of coupling between suppression
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[0024] A kind of Nb of the present invention 3 The preparation method of Al superconducting wire precursor specifically comprises the following steps:
[0025] Step 1, using Nb rods, pure Ta foil or Ta-Cu-Ta composite foils and Cu tubes to prepare single-core composite rods: centering on Nb rods, Nb foils and Al foils with a thickness ratio of 3:1 were placed on the Nb rods Coil, and then coil 1 to 3 layers of Ta-containing foil as a barrier layer; put the coiled Nb rod into a Cu tube, and perform drawing processing at a rate of 1 to 10 m per minute to obtain Nb / Al / Ta / Cu single-core composite rod or Nb / Al / Ta-Cu-Ta single-core composite rod;
[0026] Step 2, rolling the obtained single-core composite rod into a regular hexagonal hexagonal rod through a rolling process: rolling the single-core composite rod obtained through step 1 into a distance between sides of 1 to 10 mm and a length of 200 to 300 mm regular hexagonal rods, and then corrode Cu on the surface to make Nb-Al / ...
Embodiment 1
[0031] Take the Nb rod with a diameter of 8mm and a length of 300mm as the center, wind a Nb foil with a thickness of 0.3mm and an Al foil with a thickness of 0.1mm, and then roll a layer of Ta foil as a barrier layer. The diameter after winding is 23mm; The coiled Nb rod is packed into a Cu tube with an inner diameter of 24 mm and a thickness of 6 mm, and is drawn at a rate of 1 m per minute to obtain a Nb / Al / Ta / Cu single-core composite rod with a diameter of 10 mm; The Nb / Al / Ta / Cu single-core composite rod is rolled into a regular hexagonal rod with a distance of 1 mm and a length of 200 mm, and then the surface Cu is etched away to obtain a Nb-Al / Ta hexagonal rod; 144 lengths Put a 300mm hexagonal rod into a Cu-clad tube (inner diameter 36mm and thickness 6mm), and seal the Cu-clad tube by welding to obtain a composite ingot; the composite ingot is isostatically pressed under a pressure of 4000kN Processing, and then preheated to 100 ° C, and under the thrust of 4000kN, hot...
Embodiment 2
[0034]Take the Nb rod with a diameter of 8mm and a length of 300mm as the center, wind a Nb foil with a thickness of 0.3mm and an Al foil with a thickness of 0.1mm, and then roll a layer of Ta-Cu-Ta composite foil as a barrier layer, and wind The final diameter is 23mm; the coiled Nb rod is packed into a Cu tube with an inner diameter of 24mm and a thickness of 6mm, and is drawn at a rate of 3m per minute to obtain a Nb / Al / Ta- Cu-Ta single-core composite rod; Nb / Al / Ta-Cu-Ta single-core composite rod is rolled into a regular hexagonal rod with a distance across sides of 6mm and a length of 250mm, and then the surface Cu is etched away to obtain Nb -Al / Ta-Cu-Ta hexagonal rods; put 61 hexagonal rods with a length of 200mm into the Cu cladding tube (36mm inner diameter and 6mm thickness), and seal the Cu cladding tube by welding to obtain a composite billet Ingot: The composite ingot is subjected to isostatic pressing under a pressure of 4500kN, then preheated to 150°C, and under ...
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