Sodium cumenesulfonate solution and preparation method thereof
A technology of sodium cumene sulfonate and cumene, applied in the direction of sulfonic acid preparation, sulfonate preparation, chemical instruments and methods, etc., can solve the problems of poor product quality, waste of raw materials, low efficiency, etc., and achieve saving of raw materials , Improve production efficiency and reduce costs
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Embodiment 1
[0021] A kind of preparation method of sodium cumene sulfonate solution, concrete preparation steps are as follows:
[0022] Add 1.96t of 98% concentrated sulfuric acid to 3.84t of cumene at a constant speed under rapid stirring conditions, and react at 100°C. The cumene and the generated water are azeotroped, and the generated water is removed by reflux. After reacting for 6 hours, the amount of generated water is 354.64 kg. 1.44t of unreacted cumene was separated by vacuum distillation and collected for reuse.
[0023] Add 3.95 t of 20% sodium hydroxide solution to the reacted product under rapid stirring conditions to neutralize the product, and the content of sodium cumene sulfonate is 40.68%.
[0024] Control the temperature of the product at 45°C, add 308.22 kg of 30% hydrogen peroxide under stirring, and bleach for 2 hours.
Embodiment 2
[0026] A kind of preparation method of sodium cumene sulfonate solution, concrete preparation steps are as follows:
[0027] Add 0.72t of 98% concentrated sulfuric acid to 1.41t of cumene at a constant speed under rapid stirring conditions, and react at 110°C. The cumene and the generated water are azeotroped, and the generated water is removed by reflux. After 6 hours of reaction, the amount of generated water is 131.83kg. 0.53t of unreacted cumene was separated by vacuum distillation and collected for reuse.
[0028] Add 1.47t of 20% sodium hydroxide solution to the reacted product under rapid stirring condition to neutralize the product, and the content of sodium cumene sulfonate is 40.57%.
[0029] The temperature of the product was controlled at 45° C., 101.84 kg of 30% hydrogen peroxide was added under stirring, and bleached for 2 hours.
Embodiment 3
[0031] A kind of preparation method of sodium cumene sulfonate solution, concrete preparation steps are as follows:
[0032] Add 1.12t of 98% concentrated sulfuric acid to 2.19t of cumene at a constant speed under rapid stirring conditions, react at 105°C, cumene and generated water azeotrope, reflux to remove the generated water, react for 6h, the amount of generated water 205.52kg. 0.826t of unreacted cumene was separated by vacuum distillation and collected for reuse.
[0033] Add 2.28 t of 20% sodium hydroxide solution to the reacted product under rapid stirring condition to neutralize the product, and the content of sodium cumene sulfonate is 40.61%.
[0034] The temperature of the product was controlled at 45° C., and 152.40 kg of 30% hydrogen peroxide was added under stirring for 2 hours of bleaching.
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